超声法制备纳米氧化镍其性能研究 |
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引用本文: | 罗元庆,;韩永朝,;魏娜,;张绍辉,;孙万虹.超声法制备纳米氧化镍其性能研究[J].西北民族学院学报,2014(1):27-31. |
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作者姓名: | 罗元庆 ;韩永朝 ;魏娜 ;张绍辉 ;孙万虹 |
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作者单位: | [1]西北民族大学化工学院,甘肃兰州730030; [2]西北民族大学实验中心,甘肃兰州730030 |
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基金项目: | 国家级大学生创新创业训练计划项目(2013011);2012年、2013年西北民族大学开放实验项目经费资助;西北民族大学中央高校基本科研业务费资助(31920130025). |
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摘 要: | 采用不同方法制备了超级电容器材料NiO纳米球.运用XRD、SEM和TEM对制备的NiO进行了形貌和结构分析.结果表明:在表面活性剂SDBS存在下,超声法制备的NiO为球状结构,粒径为13nm.在-0.43nm.在-0.40.6V的电位范围内,NiO-US表现出典型的法拉第准电容特性.
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关 键 词: | 氧化镍 超声法 超级电容器 |
Synthesis and Characterization of NiO Nanospheres with Ultrasonic Method |
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Institution: | LUO Yuan-qing, HAN Yong-chao, WEI Na, ZHANG Shao-hui, SUN Wan_hong (Chemical Engineering College of Northwest University for Nationalities, Lanzhou 730030, China; 2. Center o{ Experiment, Northwest University for Nationalities, Lanzhou 730030, China) |
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Abstract: | NiO nanosphere for supercapacitors was prepared using different methods. The morphology and structure of samples were analyzed by X- ray diffraetion(XRD), scanning electron microscopy(SEM) and transmission electron microscopy (TEM). The results showed that the prepared samples with the ultrasound method in the presence of a surfactant (SDBS) were nanosphere and the average diameter of NiO nanospheres is only 1 - 3 nm. Within the potential range of - 0.4--0.6 V, NiO - US showed a typical quasi -Faraday capacitance characteristics. |
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Keywords: | Nickel oxide Ultrasonic method Supercapacitors |
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