| 高效液相色谱法测定氟虫腈 |
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| 引用本文： | 张云升,李志伟.高效液相色谱法测定氟虫腈[J].河北省科学院学报,2010,27(2):40-42. |
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| 作者姓名： | 张云升 李志伟 |
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| 作者单位： | 1. 河北爱尔海泰制药有限公司,河北,石家庄,050035
2. 河北科技大学化学与制药工程学院,河北,石家庄,050018 |
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| 摘 要： | 用高效液相色谱对氟虫腈的分析方法进行了研究,紫外检测器、Hypersil ODS2柱,以乙腈＋甲醇＋水为流动相（体积比为30∶40∶30）,对氟虫腈的分析可取得满意的效果。该法线性范围是0.02 mg/mL~0.60 mg/mL,最低检测限为8.0×10-8mg/mL。氟虫腈的含量为96.4%,有关物质为3.1%。
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| 关 键 词： | 氟虫腈 高效液相色谱 含量 有关物质 |
Determination of fipronil with HPLC |
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| ZHANG Yun-sheng,LI Zhi-wei.Determination of fipronil with HPLC[J].Journal of The Hebei Academy of Sciences,2010,27(2):40-42. |
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| Authors: | ZHANG Yun-sheng LI Zhi-wei |
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| Institution: | ZHANG Yun-sheng1,LI Zhi-wei2(1.Hebei Ideal & Hightech Pharmaceutical Co.,Ltd,Shijiazhuang Hebei 050035,China,2.College of Chemical and Pharmaceutical Engineering,Hebei University of Science and Technology,Shijiazhuang Hebei 050018,China) |
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| Abstract: | Method of HPLC for fipronil was studied in this article.Fipronil was determined by HPLC with UV detector,ODS column and acetonitrile＋methanol＋water as mobile phase,the results was satisfactory.Linear scope of the method is from 0.02 mg/mL to 0.60 mg/mL.The lowest detection limit is 8.0 × 10-8 mg/mL.The content and related sustance of fipronil are 96.4% and 3.1%. |
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| Keywords: | Fiprosil HPLC Analysisi Related compounds |
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