| 2-(1-苄基-1H-1,2,3-三唑-4-)吡啶及其镍(Ⅱ)配合物的合成及结构的确定 |
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| 引用本文： | 秦璐,崔杰,王聪聪,陈霞.2-(1-苄基-1H-1,2,3-三唑-4-)吡啶及其镍(Ⅱ)配合物的合成及结构的确定[J].山西大学学报(自然科学版),2011(Z2):36-38. |
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| 作者姓名： | 秦璐 崔杰 王聪聪 陈霞 |
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| 作者单位： | 山西大学化学化工学院与应用化学研究所; |
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| 基金项目： | 国家自然科学基金(21072120); 山西省科技攻关项目(20110321055) |
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| 摘 要： | 以2-乙炔基吡啶、苄基氯、叠氮化钠为原料通过Click Chemistry的方法,合成一种新的"Click"配体,并对其结构进行X-射线单晶衍射表征.再与后过渡金属NiBr2(DME)作用,合成其金属配合物,对其结构进行红外光谱、元素分析表征.
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| 关 键 词： | “Click”配体 镍(Ⅱ)配合物 铜催化 |
Synthesis and Structural Studies of 2-(1-benzyl-1H-1,2,3-triazol-4-yl)pyridine and Its Nickel(Ⅱ)Complex |
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| QIN Lu,CUI Jie,WANG Cong-cong,CHEN Xia.Synthesis and Structural Studies of 2-(1-benzyl-1H-1,2,3-triazol-4-yl)pyridine and Its Nickel(Ⅱ)Complex[J].Journal of Shanxi University (Natural Science Edition),2011(Z2):36-38. |
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| Authors: | QIN Lu CUI Jie WANG Cong-cong CHEN Xia |
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| Institution: | QIN Lu,CUI Jie,WANG Cong-cong,CHEN Xia(School of Chemistry and Chemical Engineering,Shanxi University,Taiyuan 030006,China) |
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| Abstract: | A new kind of Click ligand was prepared by the reaction of 2-Ethynylpyridine with benzyl chloride and sodium azide by way of Click Chemistry,the compound 1 was characterized by X-ray single crystal diffraction,and it was reacted with NiBr2(DME).The complexes were characterized by IR spectrum and elemental analysis. |
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