| 相转移条件下钯催化合成邻氯苯乙酸 |
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| 引用本文： | 张前军,祝荣富,赵.相转移条件下钯催化合成邻氯苯乙酸[J].贵州大学学报(自然科学版),2000,17(1):42-44. |
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| 作者姓名： | 张前军 祝荣富 赵 |
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| 作者单位： | 贵州大学化学系,贵阳,550025 |
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| 摘 要： | 报道在相转移催化剂存在下，以Ｐｄ（ＰＰｈ３）２Ｃｌ２作羰基催化剂，用邻氯氯苄、一氧化碳为原料在常压下羰基化合成邻氯苯乙酸，收率６２．２％，并考察了该反应的影响因素。
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| 关 键 词： | 邻氯苯乙酸 合成 相转移催化 钯 催化剂 |
| 文章编号： | 1000-5269(2000)01-0042-03 |
| 修稿时间： | 1999-09-16 |
Palladium Catalytic Synthesis 2-Chloro-benzeneacetic Acid Under PTC conditions |
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| Zhang Qianjun,Zhu Rongfu,Zhao Chongzhifeiyao.Palladium Catalytic Synthesis 2-Chloro-benzeneacetic Acid Under PTC conditions[J].Journal of Guizhou University(Natural Science),2000,17(1):42-44. |
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| Authors: | Zhang Qianjun Zhu Rongfu Zhao Chongzhifeiyao |
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| Institution: | Zhang Qianjun
,Zhu Rongfu
,Zhao Chongzhifeiyao
(Department of Chemieal Guizhou University, Guiyang 550025) |
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| Abstract: | 2-Chloro-benzeneacetic acid was synthesized from 2-Chlorobenzyl chlorides and CO under normal atmosphere and phase transfer catalytic conditions. The conversion was 62.2% . The influential factors of this reaction were observed. |
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| Keywords: | 2-chloro - benzeneacetic acid Synthesis 2-chlorobenzyl chlorides Phase transfer catalysis dichloro-bis(triphenyl phosphine) palladium polyethylene glycol |
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