| Angulatin E和Angulatin H的NMR数据解析 |
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| 引用本文： | 魏悦,张海艳,赵天增,范毅,朱文丽.Angulatin E和Angulatin H的NMR数据解析[J].河南科学,2011,29(7):777-782. |
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| 作者姓名： | 魏悦 张海艳 赵天增 范毅 朱文丽 |
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| 作者单位： | 1. 河南省生物技术开发中心,郑州,450002
2. 郑州大学化工学院,郑州,450052 |
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| 基金项目： | 河南省省院科技合作项目 |
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| 摘 要： | 从苦皮藤根皮中分离得到2个β-二氢沉香呋喃类多元醇酯类化合物:1β,2β-二乙酰氧基-4α,6α-二羟基-8α-异丁酰氧基-9β-苯甲酰氧基-15-异戊酰氧基-β-二氢沉香呋喃(1,Angulatin E),1β,2β,15-三乙酰氧基-4α,6α-二羟基-8α -异丁酰氧基-9β-苯甲酰氧基-β-二氢沉香呋喃(2,A...
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| 关 键 词： | NMR 归属 2D NMR 苦皮素E 苦皮素H |
Structural Elucidation of Angulatin E and Angulatin H from Celastrus Angulatus Maxim by NMR Spectroscopy |
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| Wei Yue,Zhang Haiyan,Zhao Tianzeng,Fan Yi,Zhu Wenli.Structural Elucidation of Angulatin E and Angulatin H from Celastrus Angulatus Maxim by NMR Spectroscopy[J].Henan Science,2011,29(7):777-782. |
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| Authors: | Wei Yue Zhang Haiyan Zhao Tianzeng Fan Yi Zhu Wenli |
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| Institution: | 1.Biotechnology Developing Center,Henan Academy of Sciences,Zhengzhou 450002,China;2.College of Chemical Engineering,Zhengzhou University,Zhengzhou 450052,China) |
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| Abstract: | 1β,2β-diacetoxy-4α,6α-dihydroxy-8α-isobutanoylox-9β-benzoyloxy-15-（3-methy） isobutanoyloxy-β-dihydroagrofuran（1）,1β,2β,15-triacetoxy-4α,6α-dihydrox-8α-isobutanoylox-9β-benzoylox-β-dihydroagrofuran（2） were isolated from Celastrus Angulatus Maxim.The 1H and 13C NMR chemical shifts of the compounds were completely assigned using a combination of 1D NMR（1H,13C NMR and DEPT） and 2D NMR（1H-1H COSY,HSQC and HMBC） techniques. |
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| Keywords: | NMR assignment 2D NMR Angulatin E Angulatin H |
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