| 25,26,27-三甲氧基-28-羟基杯[4]芳烃的合成 |
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| 引用本文： | 范平,山辉,曹家庆.25,26,27-三甲氧基-28-羟基杯[4]芳烃的合成[J].辽宁大学学报(自然科学版),2004,31(2):191-192. |
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| 作者姓名： | 范平 山辉 曹家庆 |
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| 作者单位： | 辽宁大学,化学科学与工程学院,辽宁,沈阳,110036 |
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| 摘 要： | 以硫酸二甲酯为烷基化试剂与杯 4 ]芳烃反应 ,合成了 2 5 ,2 6 ,2 7 三甲氧基 2 8 羟基杯 4 ]芳烃 ,通过1HNMR和IR对其结构进行了表征 .在所选合成条件下 ,标题化合物的最高收率可达 6 2 % .
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| 关 键 词： | 25 26 27-三甲氧基-28-羟基杯[4]芳烃 杯[4]芳烃 烷基化 |
| 文章编号： | 1000-5846(2004)02-0191-02 |
Synthesis of 25,26,27-Trimethoxy-28-hydro Calix[4]arene |
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| FAN Ping,SHAN Hui,CAO Jia-qing.Synthesis of 25,26,27-Trimethoxy-28-hydro Calix[4]arene[J].Journal of Liaoning University(Natural Sciences Edition),2004,31(2):191-192. |
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| Authors: | FAN Ping SHAN Hui CAO Jia-qing |
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| Abstract: | The 25,26,27-Trimethoxy-28-hydrocalixarene was synthesized by the alkylation of calixarene, and its purifying method was improved by Thin Chromatographic method. The structure of the compound was confirmed by ~1 HNMR and IR. The yield of the compound was 62%. |
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| Keywords: | Trimethoxy-28-hydrocalixarene calixarene alkylation |
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