| 高效液相色谱法测定地表灰尘中的16种多环芳烃 |
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| 引用本文： | 王娅,方志青,林野,杨成,严敏,贺华中,王雅洁.高效液相色谱法测定地表灰尘中的16种多环芳烃[J].江西师范大学学报(自然科学版),2012(3):313-316. |
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| 作者姓名： | 王娅 方志青 林野 杨成 严敏 贺华中 王雅洁 |
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| 作者单位： | 1. 贵州民族学院化学与环境科学学院,贵州贵阳550025
2. 贵州省疾病预防控制中心,贵州贵阳550004 |
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| 基金项目： | 贵州省科学技术基金([2009]2037号)资助项目 |
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| 摘 要： | 用高效液相色谱分析方法测定了地表灰尘中16种多环芳烃.样品经超声提取、硅胶萃取柱净化后,用液相色谱测定.优化了试验条件,16种多环芳烃的检出限为0.08~4.65μg/kg,方法线性关系良好,基质加标回收率为77.6%~113.7%,相对标准偏差为1.26%~7.32%
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| 关 键 词： | 多环芳烃 地表灰尘 固相萃取 高效液相色谱法 |
The Determination for 16 Polycyclic Aromatic Hydrocarbons in Surface Dust by High Performance Liquid Chromatography |
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| WANG Ya,FANG Zhi-qing,LIN Ye,YANG Cheng,YAN Ming,HE Hua-zhong,WANG Ya-jie.The Determination for 16 Polycyclic Aromatic Hydrocarbons in Surface Dust by High Performance Liquid Chromatography[J].Journal of Jiangxi Normal University (Natural Sciences Edition),2012(3):313-316. |
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| Authors: | WANG Ya FANG Zhi-qing LIN Ye YANG Cheng YAN Ming HE Hua-zhong WANG Ya-jie |
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| Institution: | 1(1.School of Chemistry and Environmental Science,Guizhou University for Nationalities,Guiyang Guizhou 550025,China;2.Guizhou Center for Disease Control and Prevention,Guiyang Guizhou 550004,China;) |
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| Abstract: | The determination method of 16 PAHs in surface dust was studied by HPLC,the samples were pretreated by ultrasonic extraction with dichlormethane and acetone as solvent,silica purification,hexane and dichlormethane washing.The results demonstrated the detection limits of method for 16 PAHs were from 0.08 to 4.65 μg/kg with good linearity,the recoveries of standard addition ranged from 77.6% to 113.7%,relative standard deviation varied between 1.26% and 7.32%. |
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| Keywords: | PAHs surface dust solid phase extraction HPLC |
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