| 顶空固相微萃取-GC-MS法分析藿香正气丸挥发性成分 |
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| 引用本文： | 张晓珊,高文华,徐严平,陈图峰,张海丹.顶空固相微萃取-GC-MS法分析藿香正气丸挥发性成分[J].汕头大学学报(自然科学版),2008,23(2):50-55. |
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| 作者姓名： | 张晓珊 高文华 徐严平 陈图峰 张海丹 |
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| 作者单位： | 汕头大学分析测试中心,广东汕头,515063 |
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| 基金项目： | 广东省汕头市科技计划
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汕头大学青年科研基金 |
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| 摘 要： | 采用顶空固相微萃取-气相色谱-质谱联用法(HS-SPME-GC-MS)分离鉴定藿香正气丸中的挥发性成分,通过筛选固相微萃取纤维,优化固相微萃取操作条件,并采用GC-MS对解析物进行分离鉴定.共鉴定出73种组分,主要为烃类倍半萜类化合物.其中,广藿香醇含量最高,为17.6%.结果表明,本实验方法适用于藿香正气丸中挥发性成分的快速分析.
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| 关 键 词： | 顶空固相微萃取 气相色谱-质谱联用 挥发性成分 藿香正气丸 |
| 文章编号： | 1001-4217(2008)02-0050-06 |
| 修稿时间： | 2007年11月30 |
HS-SPME-GC-MS for Analysis of Volatile Components from Huoxiang Zhenqi Wan |
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| ZHANG Xiao-shan,GAO Wen-hua,XU Yan-ping,CHEN Tu-feng,ZHANG Hai-dan.HS-SPME-GC-MS for Analysis of Volatile Components from Huoxiang Zhenqi Wan[J].Journal of Shantou University(Natural Science Edition),2008,23(2):50-55. |
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| Authors: | ZHANG Xiao-shan GAO Wen-hua XU Yan-ping CHEN Tu-feng ZHANG Hai-dan |
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| Institution: | (Center of Analysis and Testing of Shantou University, Shantou 515063, Guangdong, China) |
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| Abstract: | Headspace solid-phase micro-extraction（HS-SPME） technique was employed to extract the volatile compounds from Huoxiang Zhenqi Wan. The volatile components were isolated and identified successfully by gas chromatography-mass spectrometry（GC- MS）. The volatiles were collected using several SPME parameters（including extraction time and temperature）. The best response was obtained using a PDMS ＇fiber by HS- SPME when the extraction temperature was 80 ℃, extraction time was 20 min and desorption time was 5 min. Seventy-three components were identified by HS-SPME. The main components were sesquiterpenoid hydrocarbons compounds. The results showed that the HS-SPME technique can be used to extract the volatile components from HS- SPME-GC-MS. |
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| Keywords: | headspace solid-phase micro-extraction（HS-SPME） gas chromatography-mass spectrometry volatile components Huoxiang Zhenqi Wan |
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