| CP—A型微机极谱法测定发锌 |
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| 引用本文： | 姜德芝,李玉兰,李兰英.CP—A型微机极谱法测定发锌[J].高师理科学刊,1995(1). |
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| 作者姓名： | 姜德芝 李玉兰 李兰英 |
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| 作者单位： | 齐齐哈尔轻工学院(姜德芝)，齐齐哈尔市教育学院(李玉兰)，讷河市卫生防疫站(李兰英) |
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| 摘 要： | 本文研究了用CP—A型微机极谱法测定发锌的方法。本法采用HX—1型精密控温消解仪,以混酸消化样品。加入底液后,乙二胺与锌发生配合反应,配合物在滴汞电极上产生吸附催化波。发锌含量与峰电流强度呈线性关系。消化时间为90min,消化过程采用精密控温。检测限为20μg/L锌。发锌含量为97.0mg/kg时,变异系数为3.1％。加标值为100mg/kg的回收率为101.6％。
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| 关 键 词： | 锌 微量分析 毛发 极谱分析 |
Determination of Zinc in Hair by CP-A Microcomputer Polarography |
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| Jiang Dezhi,Li Yulan.Determination of Zinc in Hair by CP-A Microcomputer Polarography[J].Journal of Science of Teachers＇College and University,1995(1). |
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| Authors: | Jiang Dezhi Li Yulan |
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| Institution: | Jiang Dezhi Li Yulan(Qiqihar Light Industry Institute) (Qiqihar Education College) Li Lanying(Nehe Health Prevention Station) |
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| Abstract: | The method for the determination of zinc in hair is studied by microcomputer polarography. The HX-1 degention instrument is used to deal the sampie by mix acid. The complex that zinc is reacted with etirendaiamain is absorbed to DME and produces the calalytic wave. There is a linear relation between thecontent of hair zinc and peakhighty. digesting time is 90 minutes. Linit of determination is 0.5mg/kg. When content of hair zinc is 97. Omg/kg,coefficient of variation 3.98 percent,rate of recovery 101.6mg/kg percent. |
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| Keywords: | Zinc Micro-analysis Hair Polarographic analysis |
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