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具有波纹形貌的聚苯胺微纳米管的制备及表征
引用本文:高鑫,王冰哲,朴光哲. 具有波纹形貌的聚苯胺微纳米管的制备及表征[J]. 青岛化工学院学报(自然科学版), 2014, 0(2): 111-114
作者姓名:高鑫  王冰哲  朴光哲
作者单位:青岛科技大学橡塑材料与工程教育部重点实验室;高分子科学与工程学院,山东青岛266042
基金项目:科技部国际合作计划项目(2011DFA50430);国家自然科学基金项目(50773033);山东省自然科学基金项目(Y2007F01).
摘    要:以富勒烯C60微纳米纤维(fullerenemicro/nano fibers,FM/NFs)作为可容易移除模板,利用直接超声混合法,成功地制备了具有波纹形貌的聚苯胺微纳米管。光学显微镜观察表明,聚苯胺呈纤维状,其长度分布在2~5μm之间。扫描电镜和透射电镜观察结果表明,聚苯胺微纳米纤维形貌类似于波纹管,波纹周期约为100nm,外径在0.5~1μm之间,为空心管状结构。

关 键 词:直接超声混合法  波纹状聚苯胺微纳米管  富勒烯微纳米纤维  模板

Preparation and Characterization of Corrugated Polyaniline Micro/Nanotubes
GAO Xin,WANG Bing-zhe,PIAO Guang-zhe. Preparation and Characterization of Corrugated Polyaniline Micro/Nanotubes[J]. Journal of Qingdao Institute of Chemical Technology(Natural Science Edition), 2014, 0(2): 111-114
Authors:GAO Xin  WANG Bing-zhe  PIAO Guang-zhe
Affiliation:(Key Laboratory of Rubber-plastics, Ministry of Education, College of Polymer Science and Technology, Qingdao University of Science and Technology, Qingdao 266042, China)
Abstract:Novel corrugated polyaniline (PANI) micro/nanotubes are fabricated for the first time with fullcrene C60 micro/nano fibers (FM/NFs) as an easy removable template by direct ultrasonic mixing method. It was found that the resulting PANI has an outer diameter of 0.5--1μm and a length of 2--5 μm. Moreover, the morphology and structure of the PANI is a corrugated micro/nanotube, and the wave pitch is about 100 nm.
Keywords:direct ultrasonic mixing method  corrugated polyaniline micro/nanotubes  fullerene micro/nano fibers  template
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