| 2-己基噻吩的合成与表征 |
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| 引用本文： | 化林,杨振强,朱向珺,蒋卫鹏,王艳果.2-己基噻吩的合成与表征[J].河南科学,2011,29(6):663-665. |
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| 作者姓名： | 化林 杨振强 朱向珺 蒋卫鹏 王艳果 |
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| 作者单位： | 河南省科学院化学研究所有限公司,郑州,450002 |
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| 摘 要： | 以噻吩为原料,经Friedel-Crafts酰基化反应制得2-己酰基噻吩,然后,2-己酰基噻吩经wolf-Kishner-黄鸣龙还原反应合成了目标产物2-己基噻吩,总收率为65%以上.通过1H NMR、MS分析确证了2-己酰基噻吩与标题化合物的结构.
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| 关 键 词： | 2-己酰基噻吩 2-己基噻吩 合成与表征 |
Synthesis and Characterization of 2-Hexylthiophene |
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| Hua Lin,Yang Zhenqiang,Zhu Xiangjun,Jiang Weipeng,Wang Yanguo.Synthesis and Characterization of 2-Hexylthiophene[J].Henan Science,2011,29(6):663-665. |
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| Authors: | Hua Lin Yang Zhenqiang Zhu Xiangjun Jiang Weipeng Wang Yanguo |
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| Institution: | (Institute of Chemistry,Henan Academy of Sciences,Zhengzhou 450002,China) |
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| Abstract: | The 1-（thiophen-2-yl）-hexan-1-one was synthesized with thiophene and hexanoyl chloride as starting materials by friedel-crafts reaction,then 2-hexylthiophene was prepared via Wolf-Kishner-Huang reduction reaction from 1-（thiophen-2-yl）-hexan-1-one.The target compound 2-hexylthiophene was prepared with its total yield reaching 65 %.The structures of 1-（thiophen-2-yl）-hexan-1-one and 2-hexylthiophene were determined by 1H NMR,MS analysis. |
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| Keywords: | 1-（thiophen-2-yl）-hexan-1-one 2-hexylthiophene synthesis and characterization |
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