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毛细管区带电泳法测定中药枳实中柚皮素的含量
引用本文:刘海兴.毛细管区带电泳法测定中药枳实中柚皮素的含量[J].烟台大学学报(自然科学与工程版),2008,21(4):310-312.
作者姓名:刘海兴
作者单位:潍坊学院化学化工系,山东,潍坊,261061;青岛科技大学化学学院,山东,青岛,266071
摘    要:采用毛细管区带电泳法测定了枳实中柚皮素的含量.在30mmol/LNa2B4O7缓冲溶液(pH=10.00)的条件下,实现了被测组分的有效分离.测得的枳实中柚皮素的含量为:0.5867mg/g,RSD=4.12%(n=4).柚皮素的平均回收率为114.7%(n=3).为中药枳实的质量控制提供了新方法.

关 键 词:毛细管区带电泳  枳实  柚皮素

Determination of Naringenin in Fructus Aurantii Immaturus by Capillary Zone Electrophoresis
LIU Hai-xing.Determination of Naringenin in Fructus Aurantii Immaturus by Capillary Zone Electrophoresis[J].Journal of Yantai University(Natural Science and Engineering edirion),2008,21(4):310-312.
Authors:LIU Hai-xing
Institution:LIU Hai-xing ( 1. Department of Chemistry and Chemical Engineering, Weifang University, Weifang 261061, China ;2. College of Chemistry, Qingdao University of Science and Technology, Qingdao 266071, China)
Abstract:The capillary zone electrophoresis is used for the determination of the content of the naringenin in Fructus Aurantii Immaturus. In 30 mmol/L Na2B4O7 buffer condition (pH = 10. 00), the component' s effective separation has been achieved. The content of naringenin in Fructus Aurantii Immaturus is 0. 5867 mg/g, RSD =4. 12% (n =4). The average recovery of naringenin is 114.7% (n =3). A new method of the quality control of Fructus Aurantii lmmaturus herb is given.
Keywords:capillary zone electrophoresis  Fructus Aurantii Imrnatizrus  naringenin
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