| 双杂原子Ti-V-ZSM-5分子筛的合成与表征 |
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| 引用本文： | 霍丽华,赵经贵,马淑杰. 双杂原子Ti-V-ZSM-5分子筛的合成与表征[J]. 黑龙江大学自然科学学报, 2001, 18(1): 82-85 |
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| 作者姓名： | 霍丽华 赵经贵 马淑杰 |
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| 作者单位： | 黑龙江大学化学化工学院,;吉林大学化学系, |
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| 基金项目： | 黑龙江省自然科学基金资助课题(9732) |
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| 摘 要： | 在无碱性离子存在下,以硅溶胶、硫酸钛、硫酸氧钒为原料,分别采用四丙基溴化胺(TPABr)、1,6-己二胺(1,6-HDA)及正丁胺(R-NH2)模板剂,首次合成了双杂原子Ti-V-ZSM-5分子筛,并对产物的物性与结构进行了表征。
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| 关 键 词： | 双杂原子 Ti-V-ZSM-5分子筛 水热合成 |
| 文章编号： | 1001-7011(2001)01-0082-04 |
| 修稿时间： | 1999-11-02 |
Synthesis and characterization of zeolite Ti-V-ZSM-5 containing double heteroatoms |
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| HUO Li-Hua,ZHAO Jing-Gui,MA Shu-jie. Synthesis and characterization of zeolite Ti-V-ZSM-5 containing double heteroatoms[J]. Journal of Natural Science of Heilongjiang University, 2001, 18(1): 82-85 |
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| Authors: | HUO Li-Hua ZHAO Jing-Gui MA Shu-jie |
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| Abstract: | The synthesis of zeolite Ti-V-ZSM-5 containing double heteroatoms with silica sol as Sisources, titanium sulfate and vandium oxisulfate as the starting materials and tetrapropyl ammonium bromide(TPABr), 1, 6-dihexamine(1,6-HDA) and n-butylamine as the templates, respectively was investigated for the first time in the absence of alkali metal ions. Some physical and chemical properties and the structure of the product were characterized by using XRD, SEM, TG-DTA, IR, UV-Vis spectra. |
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| Keywords: | double heteroatom Ti-V-ZSM-5 zeolite hydrothermal synthesis |
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