| 微波辐射六氢吡啶催化快速合成乙酰水杨酸的研究 |
| |
| 引用本文： | 赵士举,金秋,苏惠,李伟,徐翠莲. 微波辐射六氢吡啶催化快速合成乙酰水杨酸的研究[J]. 应用科技, 2010, 37(1): 53-56 |
| |
| 作者姓名： | 赵士举 金秋 苏惠 李伟 徐翠莲 |
| |
| 作者单位： | 河南农业大学,理学院,河南,郑州,450002 |
| |
| 基金项目： | 国家科技攻关基金资助项目 |
| |
| 摘 要： | 以水杨酸和乙酸酐为原料,微波辐射加热,六氢吡啶为催化剂,快速合成了乙酰水杨酸.通过正交试验及直观分析,探索出了最佳合成工艺条件;通过方差分析,得出了影响次序和程度.该方法为高效、环保、低能合成乙酰水杨酸提供了新的工艺条件.
|
| 关 键 词： | 乙酰水杨酸 微波 六氢吡啶 合成 正交试验 |
Research on rapid synthesis of acetylsalicylic acid catalysed by piperidine under microwave radiation |
| |
| ZHAO Shi-ju,JIN Qiu,Su Hui,LI Wei,XU Cui-lian. Research on rapid synthesis of acetylsalicylic acid catalysed by piperidine under microwave radiation[J]. Applied Science and Technology, 2010, 37(1): 53-56 |
| |
| Authors: | ZHAO Shi-ju JIN Qiu Su Hui LI Wei XU Cui-lian |
| |
| Affiliation: | ( College of Science, Henan Agricultural University, Zhengzhou 450002, China) |
| |
| Abstract: | The acetylsalicylic acid was synthesized rapidly piperidine, and heated by microwave radiation. Through th dition of synthesis process was concluded, and the sequenc from salicylic acid and acetic anhydride, catalysed by e orthogonal test and intuitive analysis, the optimal con- e and degree of the influence on yield were educed from the variance analysis. This paper provides a new synthesis process which is highly efficient, environmentally beneficial, and low energy-consuming. |
| |
| Keywords: | acetylsalicylic acid microwave piperidine synthesis orthogonal test |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
