| 5-硝基糠叉二醋酸酯的制备 |
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| 引用本文： | 李慧章,高木欣.5-硝基糠叉二醋酸酯的制备[J].河北大学学报(自然科学版),1992(3). |
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| 作者姓名： | 李慧章 高木欣 |
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| 作者单位： | 河北大学化学系
(李慧章)，河北大学化学系(高木欣) |
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| 摘 要： | 本文介绍了5—硝基糠叉二醋酸酯的制备方法。讨论了不同硝化体系对收率的影响,实验表明,发烟硝酸作为硝化剂收率最高。
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| 关 键 词： | 5-硝基糠叉二醋酸酯 制备 糠醛 硝化 |
Preparation of 5-Nitrofurfurylidene Diacetate |
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| LI Huizhang Gao Muxin.Preparation of 5-Nitrofurfurylidene Diacetate[J].Journal of Hebei University (Natural Science Edition),1992(3). |
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| Authors: | LI Huizhang Gao Muxin |
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| Institution: | Department of Chemistry |
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| Abstract: | The title compound was prepared by nitration of furfural with five kinds of nitration systems ( fuming HNO3, Ac2O; HNO3, Ac2O, SbSl3; HNO3, Ac2O, P-toluene-slfonic acid; H2SO4, NaIO3, NaNO3, Ac2O; HNO3) The highest gield was obtained in nitration with the fuming HNO3 system. |
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| Keywords: | 5-Nitrofurfurylidene diacetate Preparation Furfural Nitration |
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