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亚钛还原法测定重氮氯化锌复盐的含量
引用本文:蒋昌翎. 亚钛还原法测定重氮氯化锌复盐的含量[J]. 湖南师范大学自然科学学报, 1988, 0(3)
作者姓名:蒋昌翎
作者单位:湖南师范大学化学系
摘    要:
本文阐述了用改进的亚钛还原法,测定本单位试制的一种新的重氮感光试剂——3-甲基-4-吡咯啶基苯重氮氯化锌复盐的含量,结果为98.78%。

关 键 词:重氮盐  氯化锌复盐  重氮感光材料  亚钛还原法

THE DETERMINATION OF CONTENT OF DIAZONIUM SALT IN TITANOMETRY
Jiang Changling. THE DETERMINATION OF CONTENT OF DIAZONIUM SALT IN TITANOMETRY[J]. Journal of Natural Science of Hunan Normal University, 1988, 0(3)
Authors:Jiang Changling
Affiliation:Jiang Changling Department of Chemistry
Abstract:
In this paper,the convenient condition ofanalys is is expounded,when we usetitanometry to determine the content of diazonium salt in semifinished product:wetake in the order of operation that the sample is put in the titanium trichloridesolution slowly;the quantity of titanium trichloride is in excess of 200% or so;the time of reaction is 20 minute.Using this method,the content of 3-methyl-4-pyrrolidinyl benzene diazonium zine chloride,a new diazo light sensitive agent,is determined accuratly.It is 98.78%.
Keywords:diazonium salt  zine chloride double salt  diazo light sensitive material  titanometry
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