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| TCBA阻燃性环氧树脂合成研究 | |
| 引用本文： | 林吉文. TCBA阻燃性环氧树脂合成研究[J]. 南京理工大学学报(自然科学版), 1991, 0(3) |
| 作者姓名： | 林吉文 |
| 作者单位： | 华东工学院化工学院 |
| 摘 要： | 本文提出以1,1,1-三氯乙烷与水为混合溶剂,以RS为催化剂,由双酚A(BA)氯化合成四氯双酚A(TCBA)的合成路线,并提出经两步法由TCBA合成TCBA阻燃性环氧树脂的方法。经由正交实验与验证实验分别提出了两者合成的优化反应条件。研究结果的数据显示上述合成具有良好的重现性。 |
| 关 键 词： | 氯化 缩合反应 阻燃剂 |
A Study of Synthesis of TCBA Fireproof Epoxy Resin. |
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| Lin Jiwen Chemical Engineering School. A Study of Synthesis of TCBA Fireproof Epoxy Resin.[J]. Journal of Nanjing University of Science and Technology(Nature Science), 1991, 0(3) | |
| Authors: | Lin Jiwen Chemical Engineering School |
| Affiliation: | Lin Jiwen Chemical Engineering School |
| Abstract: | This article introduced a synthetic way on chlorination ofbisphenol A using 1, 1, 1- trichloroethane/water simultaneously as a mixedsolvent,RS as a catalyst and synthesized TCBA fireproof epoxy resin viatwo steps method. The optimum reaction conditions of synthesizing both ofthem have been offered by means of crossing tests and examinatorial ex-periments. Good repetitions of the said syntheses have been revealed by re-search data. |
| Keywords: | chlorination condensation reaction fireproofing agent |
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