| 含氢化诺卜基的叔胺类化合物的合成与结构分析 |
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| 引用本文： | 陈金珠,肖转泉,徐丽锋,王宗徳,韩招久. 含氢化诺卜基的叔胺类化合物的合成与结构分析[J]. 江西师范大学学报(自然科学版), 2016, 40(2): 179-182 |
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| 作者姓名： | 陈金珠 肖转泉 徐丽锋 王宗徳 韩招久 |
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| 作者单位： | 1.江西农业大学理学院,江西 南昌 330045; 2.江西师范大学化学化工学院,江西 南昌 330027; 3.江西农业大学林学院,江西 南昌 330045; 4.南京军区军事医学研究所,江苏 南京 210002 |
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| 摘 要： | 由cis-氢化诺卜醇与亚硫酰氯反应制得cis-氢化诺卜基氯,再分别与二甲胺、二乙胺、二正丙胺、二正丁胺、六氢吡啶、吗啉等仲胺反应,合成了6种cis-氢化诺卜基的叔胺,产品GC纯度达95%以上.通过红外光谱、核磁共振谱和质谱分析表征了它们的结构
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| 关 键 词： | 氢化诺卜醇 氢化诺卜基氯 叔胺 合成 结构分析 |
The Synthesis and Structural Analysis of Hydronopyl Tertiary Amine Compounds |
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| CHEN Jinzhu,XIAO Zhuanquan,XU Lifeng,WANG Zongde,HAN Zhaojiu. The Synthesis and Structural Analysis of Hydronopyl Tertiary Amine Compounds[J]. Journal of Jiangxi Normal University (Natural Sciences Edition), 2016, 40(2): 179-182 |
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| Authors: | CHEN Jinzhu XIAO Zhuanquan XU Lifeng WANG Zongde HAN Zhaojiu |
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| Affiliation: | 1.College of Science,Jiangxi Agricultural University,Nanchang Jiangxi 330045,China; 2.College of Chemistry,Jiangxi Normal Univesrity,Nanchang Jiangxi 330027,China; 3.College of Forestry,Jiangxi Agricultural University,Nanchang Jiangxi 330045,China; 4.Military Medical Institute of Nanjing Command,Nanjing Jiangsu 210002,China |
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| Abstract: | Cis-hydronopyl chloride was synthesized by cis-hydronopol and thionyl chloride.Then six kinds of cis-hydronopyl tertiary amine compounds were synthesized from the reaction of hydronopyl chloride with dimethylamine,diethylamin,diisopropylamin,dipropylamine,dibutylamine,hexahydropyridine and morpholine respectively.The GC content of the products were over 95% and their structures were characterized and analyzed by IR,NMR and MS methods. |
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| Keywords: | hydronopol hydronopyl chloride tertiary amine synthesis sturctural analysis |
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