| 从航煤酸渣中制取石油亚砜 |
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| 引用本文： | 郭玉美.从航煤酸渣中制取石油亚砜[J].中国石油大学学报(自然科学版),1987(2). |
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| 作者姓名： | 郭玉美 |
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| 作者单位： | 华东石油学院有机化学教研室 |
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| 摘 要： | 本文研究从航煤酸渣中制取石油亚砜的方法。将酸渣稀释,从中分出油层,用过氧化氢氧化油层得到石油亚砜。文中探讨了氧化过程中氧化剂(过氧化氢)、催化剂(冰乙酸)及反应时间对石油亚砜收率的影响。研究结果表明,氧化剂过氧化氢以1.0 mol为宜;催化剂冰乙酸的用量以0.5 mol为宜;反应时间以30分钟为宜。反应时间越长,转化率反而降低。
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| 关 键 词： | 煤油 亚砜 酸渣 氧化剂 催化剂 硫酸 |
PREPARATION OF PETROLEUM SOLFOXIBE FROM ACID SLUDGE OF AVIATION KEROSENE |
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| Guo Yumei.PREPARATION OF PETROLEUM SOLFOXIBE FROM ACID SLUDGE OF AVIATION KEROSENE[J].Journal of China University of Petroleum,1987(2). |
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| Authors: | Guo Yumei |
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| Abstract: | In this paper the preparation of petroleum sulfoxide from the acid sludge of aviation kerosene has been studied. The acid sludge was diluted and the oil layer was separated from the acid sludge. The petroleum sulfoxide can be obtained by oxidizing the oil layer with hydrogen peroxide. In the oxidation process the affects of the oxidant, the catalyst and the reaction time on the yield of petroleum sulfoxide were examined. |
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| Keywords: | Kerosene Sulfoxide Acid sludge Oxidant Catalyst sulfur ether |
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