| 三聚体二苯基锗氧化合物的合成及晶体结构研究 |
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| 引用本文： | 张如芬,张文圣,朱德中,尹汉东,马春林. 三聚体二苯基锗氧化合物的合成及晶体结构研究[J]. 聊城大学学报(自然科学版), 2001, 14(1): 13-14 |
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| 作者姓名： | 张如芬 张文圣 朱德中 尹汉东 马春林 |
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| 作者单位： | 聊城师范学院化学化工学院,山东,聊城,252059;德州学院,化学系,德州,253000 |
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| 基金项目： | 山东省自然科学基金!项目 ( Q98B0 1 1 1 7) |
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| 摘 要： | 研究了用二苯基二氯化锗的水解反应,得到了三聚体二苯基锗氧化合物,用X-射线晶体衍射确定了结构.配合物为单斜晶体,空间群P21/c.晶体学数据a=1.0018(2),b=1.862 4(4),c=1.770 9(4)nm,β=93.49(3)0,V=3 304.0(11)nm3,Z=4,Dcal.=1.464mg/m3,F(000)=1 464,R1=0.043 8,wR2=0.073.
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| 关 键 词： | 二苯基锗氧 配合物 晶体结构 |
Synthesis and CrystalStructure of Containing Germanium and Oxygen Atoms Heterocyclic Tripolymer (Ph2GeO)3 |
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| ZHANG Ru-fen,ZHANG Wen-sheng,ZHU De-zhong,YIN Han-dong,MA Chun-lin. Synthesis and CrystalStructure of Containing Germanium and Oxygen Atoms Heterocyclic Tripolymer (Ph2GeO)3[J]. JOURNAL OF LIAOCHENG UNIVERSITY (NATURAL SCIENCE, 2001, 14(1): 13-14 |
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| Authors: | ZHANG Ru-fen ZHANG Wen-sheng ZHU De-zhong YIN Han-dong MA Chun-lin |
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| Affiliation: | ZHANG Ru fen 1) ZHANG Wen sheng 2) ZHU De zhong 1) YIN Handong 1) MA Chun lin 1) |
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| Abstract: | The tripolymer compound (Ph 2GeO) 3 has been synthesized with a novel method and characterized by means of X|ray single crystal diffraction.The structure features of the compound are described. |
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| Keywords: | tripolymer diphenylgerimanium crystal structure |
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