| 微波促进下芳香醛与环缩酮的反应的研究 |
| |
| 引用本文： | 康丽琴,王红,金东元.微波促进下芳香醛与环缩酮的反应的研究[J].上海应用技术学院学报,2005,5(4):259-261. |
| |
| 作者姓名： | 康丽琴 王红 金东元 |
| |
| 作者单位： | 上海应用技术学院化学工程系,上海200235 |
| |
| 摘 要： | 用Lewis酸催化芳香醛与环缩酮进行反应，合成得到了7种环烷酮类化合物。与常规条件下的反应进行比较，结果表明在微波辐射下反应速度快，条件温和，不需要溶剂，得到的产品产率达80％。并对合成所得的7种化合物的结构通过IR和^1HNMR谱进行了表征。
|
| 关 键 词： | 芳香醛 环缩酮 Lewis酸 微波辐射 |
| 文章编号： | 1671-7333(2005)04-0259-03 |
| 收稿时间： | 2005-09-21 |
| 修稿时间： | 2005年9月21日 |
Research on Reaction of Aromatic Aldehyde and Ketal under Microwave Irradiation |
| |
| KANG Li-qin, WANG Hong ,JIN Dong-yuan.Research on Reaction of Aromatic Aldehyde and Ketal under Microwave Irradiation[J].Journal of Shanghai Institute of Technology: Natural Science,2005,5(4):259-261. |
| |
| Authors: | KANG Li-qin WANG Hong JIN Dong-yuan |
| |
| Institution: | Department of Chemical Engineering, Shanghai Institute of Technology, Shanghai 200235 ,China |
| |
| Abstract: | We have got seven kinds of cycloalkanone from aromatic aldehydes and ketals by using Lewis acid as catalyst under microwave irradiation. With respect to conventional methods, the reaction has the following advantages: short reaction time, mild reaction conditions, no solvent and in high yields. The construction of these compounds have been characterised by IR and ~1HNMR. |
| |
| Keywords: | aromatic aldehyde ketal Lewis acid microwave irradiation |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
