| 工业用1,8-二氮双环(5.4.0)-7-十一烯中水分含量的测定——气相色谱法 |
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| 引用本文： | 陶占辉,刘志红,魏巍,徐少敏.工业用1,8-二氮双环(5.4.0)-7-十一烯中水分含量的测定——气相色谱法[J].吉林工学院学报,2007,28(2):148-150. |
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| 作者姓名： | 陶占辉 刘志红 魏巍 徐少敏 |
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| 作者单位： | 吉林省石油化工设计研究院 吉林长春130021(陶占辉，魏巍，徐少敏)，长春医学高等专科学校药学系 吉林长春130031(刘志红) |
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| 摘 要： | 应用气相色谱法,选择热导池检测器,高分子多孔微球GDX-102为固定相,通过制备苯-水平衡液,以水在苯中不同温度下的溶解度为依据,对1,8-二氮双环(5.4.0)-7-十一烯样品进行测定,该方法简便、快速、可靠。
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| 关 键 词： | 气相色谱法 固定相 TCD检测器 1 8-二氮双环(5.4.0)-7-十一烯 苯-水平衡液 |
| 文章编号： | 1006-2939（2007）02-0148-03 |
| 收稿时间： | 2007-02-12 |
| 修稿时间： | 2007-02-12 |
Water content measurement in 1,8-DiazaBicyclo(5.4.0)-Undec7-ene of industry——gas chromatography |
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| TAO Zhan-hui,LIU Zhi-hong,WEI Wei,XU Shao-min.Water content measurement in 1,8-DiazaBicyclo(5.4.0)-Undec7-ene of industry——gas chromatography[J].Journal of Jilin Institute of Technology,2007,28(2):148-150. |
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| Authors: | TAO Zhan-hui LIU Zhi-hong WEI Wei XU Shao-min |
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| Institution: | 1. Jilin Province Design and Research Institute for Petrochemical Engineering, Changchun 130021, China; 2. Department of Medicine, Changchun College of Medical Training, Changchun 130031, China |
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| Abstract: | With gas chromatography,TCD as detector,macromolecular lacunaris microball as GDX-102 as stationary phase,the benzene-water balance solution is prepared to measure the.1,8-DiazaBicyclo(5.4.0)-Undec-7-ene sample based on the solubility of water in benzene at different temperature.The method is simple and realizable. |
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| Keywords: | gas chromatogram method stationary phase TCD detector 1 8-DiazaBicyclo(5 4 0)-Undec-7-ene benzene-water balanced solution |
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