| 3-(2-溴-4,5-二甲氧基苯基)丙酸异丙酯的合成 |
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| 引用本文： | 尹丽华,初飞,杨晴来,陈林. 3-(2-溴-4,5-二甲氧基苯基)丙酸异丙酯的合成[J]. 云南民族大学学报(自然科学版), 2011, 20(4): 284-286. DOI: 10.3969/j.issn.1672-8513.2011.04.012 |
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| 作者姓名： | 尹丽华 初飞 杨晴来 陈林 |
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| 作者单位： | 云南民族大学民族药资源化学国家民委-教育部重点实验室,云南昆明,650031 |
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| 摘 要： | 以3,4-二甲氧基苯丙酸为原料,经溴代、酰化、醇解反应合成了未见报道的丹参素类似物3-(2-溴-4,5-二甲氧基苯基)丙酸异丙酯,用IR、1H NMR、13C NMR谱对产物进行了表征.
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| 关 键 词： | 3,4-二甲氧基苯丙酸 3-(2-溴-4,5-二甲氧基苯基)丙酸异丙酯 合成 |
Synthesis of Isopropyl 3 - (2 - Bromo - 4,5 - Dimethoxyphenyl) Propanoate |
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| YIN Li-hua,CHU Fei,YANG Qing-lai,CHEN Lin. Synthesis of Isopropyl 3 - (2 - Bromo - 4,5 - Dimethoxyphenyl) Propanoate[J]. Journal of Yunnan Nationalities University:Natural Sciences Edition, 2011, 20(4): 284-286. DOI: 10.3969/j.issn.1672-8513.2011.04.012 |
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| Authors: | YIN Li-hua CHU Fei YANG Qing-lai CHEN Lin |
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| Affiliation: | YIN Li-hua,CHU Fei,YANG Qing-lai,CHEN Lin(Key Laboratory of Ethnic Medicine Resource Chemistry,State Ethnic Affairs Commission & Ministry of Education,Yunnan University of Nationalities,Kunming 650031,China) |
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| Abstract: | Isopropyl 3-(2-bromo-4,5-dimethoxyphenyl) propanoat was synthesized with 3-(3,4-Dimethoxyphenyl)Propionic Acid by bromination,acylation and alcoholysis reaction.Their structures were characterized by 1H NMR,13C NMR and IR. |
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| Keywords: | 3-(3 4-Dimethoxyphenyl) Propionic Acid isopropyl 3-(2-bromo-4 5-dimethoxyphenyl) propanoat synthesis |
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