Microstructure characterization of a pressureless infiltrating oxidized SiCp preform by Al-8Mg |
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Authors: | Shu-bin Ren Xiao-yu Shen Xin-bo He Xuan-hui Qu |
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Institution: | 1.School of Materials Science and Engineering,University of Science and Technology Beijing,Beijing,China |
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Abstract: | The microstructure of a pressureless infiltrating 55vol% oxidized SiC preform by Al-8Mg alloy was characterized by transmission
electron microscopy (TEM), high resolution TEM (HRTEM), field emission scanning electron microscopy (FE-SEM), and X-ray diffraction.
The TEM image of the interface between Al and SiC shows that the surface of SiC is covered by a rough nanocrystal layer of
MgAl2O4, Al2O3, and Si, produced by the interfacial reaction of Al, Mg, and SiO2 on the surface of SiC. The Al-SiC interface is also examined by HRTEM to be better understood how MgAl2O4 and Al2O3 are produced. Dendritic Al2O3 crystals are embedded in the pores of the composite generated from the mutual bonding of SiO2 on the surface of SiC. Columnar AlN crystals of about 250 nm in length are bunched vertically on the SiC particle surface. |
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