| 固体超强酸TiO_2/SO_4~(2-)催化合成苯氧乙酸烯丙酯 |
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| 引用本文： | 邵宗龙,曾雪珊.固体超强酸TiO_2/SO_4~(2-)催化合成苯氧乙酸烯丙酯[J].安徽大学学报(自然科学版),1996(1). |
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| 作者姓名： | 邵宗龙 曾雪珊 |
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| 作者单位： | 安徽大学化学系，安徽省建材工业学校 合肥 230039，合肥 230051 |
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| 摘 要： | 用TiO_2/SO_4~(2-)固体超强酸催化苯氧乙酸与烯丙醇的酯化反应,研究分析了反应因素对酯化反应产率的影响;最佳反应条件下,产物收率可达86.0％.
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| 关 键 词： | 固体超酸 苯氧乙酸 烯丙醇 苯氧乙酸烯丙酯 |
Synthesis of Allyl Phenoxyacetate with TiO_2/SO_4~(2-) Solid Superacid Catalyst |
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| Shao Zonglong Zeng Xieshan.Synthesis of Allyl Phenoxyacetate with TiO_2/SO_4~(2-) Solid Superacid Catalyst[J].Journal of Anhui University(Natural Sciences),1996(1). |
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| Authors: | Shao Zonglong Zeng Xieshan |
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| Institution: | Department of Chemistry Anhui University Hefei 230039 |
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| Abstract: | Allyl phenoxyacetate was synthesized by phenoxyacetic acid and allyl alcohol with TiO2/SO42- solid superacid catalyst. The effects of molar ratio, reaction time. Using quantity of catalyst and solvent on the product yield from the esterification reaction have been inevestigated, and the optimum reaction conditions have been found. Under the optimum reaction conditions used, the yield of allyl phenoxyacetate could reach 86.0%. |
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| Keywords: | solid superacid phenoxyacetic acid allyl alcohol allyl phenoxyacetate |
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