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铜包石墨粉体的制备及表征
引用本文:毕建聪,毕丽萍.铜包石墨粉体的制备及表征[J].黑龙江科技学院学报,2014,24(5):496-499.
作者姓名:毕建聪  毕丽萍
作者单位:1. 黑龙江科技大学材料科学与工程学院,哈尔滨,150022
2. 长春市城市科学研究所,长春,130042
基金项目:哈尔滨市科技局科技创新人才研究专项资金项目
摘    要:为简化铜包石墨粉体的制备工艺,提高镀铜质量,选用固定碳质量分数大于99%的天然石墨粉作为原料,在镀液组成确定的前提下,采用自行设计的电镀装置进行超声电镀,制备铜包石墨复合粉体.利用SEM对粉体的微观形貌进行表征.结果表明,超声施镀60 min,能较好地解决石墨颗粒的团聚问题,改善镀铜效果;铜呈细小颗粒状聚集附着在石墨的表面,包覆效果良好.该研究为铜包石墨粉体制备提供了新方法.

关 键 词:铜包石墨粉  超声电镀  微观形貌

Preparation and characterization of Cu-coated graphite powders
BI Jiancong,BI Liping.Preparation and characterization of Cu-coated graphite powders[J].Journal of Heilongjiang Institute of Science and Technology,2014,24(5):496-499.
Authors:BI Jiancong  BI Liping
Institution:BI Jiancong , BI Liping( 1. School of Materials Science & Engineering, Heilongjiang University of Science & Technology, Harbin 150022, China; 2. Changehun Institute of Urban Science, Changehun 130042, China)
Abstract:This paper is an effort to study the simplification of the preparation techniques of Cu-coa- ted graphite powder and improvement in the quality of copperizing. The research consists of using raw materials formed by natural graphite powder with fixed carbon content greater than 99%, determining the composition of plating solution, preparing Cu-coated graphite powder using self-designed electroplating apparatus tailored for ultrasonic electroplating, and characterizing the micro morphology of the powders by SEM. The results show that ultrasonic plating 60 rain affords a better solution to the agglomeration of graphite particles, contributing to the improved copper plating; copper exhibits a finer granular aggregates attached on the surface of graphite, producing a better coating effect. This study would serve as a new method for the preparation of Cu-coated graphite powder.
Keywords:Cu-coated graphite powders  ultrasonic electroplating  micro morphology
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