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| 十六胍亚硫酸盐的制备研究 | |
| 引用本文： | 陈田田,王锦堂,韦长梅.十六胍亚硫酸盐的制备研究[J].淮阴师范学院学报(自然科学版),2009,8(4):318-321. |
| 作者姓名： | 陈田田 王锦堂 韦长梅 |
| 作者单位： | 1. 南京工业大学,理学院应用化学系,江苏,南京,210009;淮阴师范学院,化学化工学院,江苏,淮安,223300 2. 南京工业大学,理学院应用化学系,江苏,南京,210009 3. 淮阴师范学院,化学化工学院,江苏,淮安,223300;江苏省低维材料化学重点建设实验室,江苏,淮安,223300 |
| 基金项目： | 江苏省教育厅自然科学基金项目，江苏省化学重点建设实验室基金项目 |
| 摘 要： | 研究了以十六胺和三氧化硫脲为原料制备十六胍亚硫酸盐的方法.通过考察反应时间、温度和物料比等因素对产物收率影响的实验,获得了优化反应条件为:以95%乙醇为溶剂,7.85g十六胺和3.10g三氧化硫脲于50℃反应2 h,产品收率可达75.91%.目标产品通过了红外、质谱和核磁共振碳谱表征. |
| 关 键 词： | 十六胺 三氧化硫脲 十六胍亚硫酸盐 |
Study on the Preparation of Hexadecylguanidium sulfite |
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| CHEN Tian-tian,WANG Jin-tang,WEI Chang-mei.Study on the Preparation of Hexadecylguanidium sulfite[J].Journal of Huaiyin Teachers College(Natrual Science Edition),2009,8(4):318-321. | |
| Authors: | CHEN Tian-tian WANG Jin-tang WEI Chang-mei |
| Abstract: | The preparation methods of hexadecylguanidium sulfite from hexadecylamine and aminoiminomethanesulfonic acid was studied.The infections of reaction temperature,time and molar ratio on the reaction yield were researched.The optimum synthesis conditions for title compound were obtained as follows: 7.85g hexadecylamine and 3.10g aminoiminomethanesulfonic acid reactied for 2 h at 50℃ in the solvent of ethanol with the yield of 75.91%.The target compound was characterized by IR,MSand 13C-NMR. |
| Keywords: | hexadecylamine aminoiminomethanesulfonic acid hexadecylguanidium sulfite |
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