| 几种新型苯甲酰基脲类几丁质抑制剂的合成(Ⅰ) |
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| 引用本文： | 严胜骄,林军,杨丽娟,黄荣,张征. 几种新型苯甲酰基脲类几丁质抑制剂的合成(Ⅰ)[J]. 云南大学学报(自然科学版), 2003, 25(6): 525-527,530 |
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| 作者姓名： | 严胜骄 林军 杨丽娟 黄荣 张征 |
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| 作者单位： | 1. 云南大学,应用化学系,云南,昆明,650091;南开大学,元素有机化学研究所,南开大学,元素有机化学国家重点实验室,天津,300071
2. 云南大学,应用化学系,云南,昆明,650091 |
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| 基金项目： | 云南省自然科学基金资助项目(1999B0005M)，南开大学元素有机化学国家重点实验室开放基金资助项目. |
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| 摘 要： | 以百菌清和卤代苯腈为原料经3～4步反应合成出2类共4个新型苯甲酰基脲类几丁质合成抑制剂6a-c和9a.两条路线的反应条件均温和,产率高.化合物的结构得到IR,MS,1HNMR,13CNMR,19FNMR,HRMS等波谱的证实.
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| 关 键 词： | 苯甲酰基脲 几丁质抑制剂 合成 |
| 文章编号： | 0258-7971(2003)06-0525-03 |
Synthesis of some novel benzoylphenylurea chitin inhibitors(Ⅰ) |
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| YAN Sheng-jiao,LIN Jun,YANG Li-Juan,HUANG Rong,ZHANG Zheng. Synthesis of some novel benzoylphenylurea chitin inhibitors(Ⅰ)[J]. Journal of Yunnan University(Natural Sciences), 2003, 25(6): 525-527,530 |
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| Authors: | YAN Sheng-jiao LIN Jun YANG Li-Juan HUANG Rong ZHANG Zheng |
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| Affiliation: | 1. Department of Applied Chemistry, Yunnan University, Kunming 650091, China;2. State Key Laboratory of Elemento-organic Chemistry, Nankai University, Tianjin 300071, China |
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| Abstract: | Four novel benzoylphenylurea chitin inhibitor derivatives 6a-c and 9,which belonging to two kind of compounds,have been synthesized from readily available starting material chlorothalonil 4 and halo benzenenitrile 1 via three to four steps.Two synthesis routes have some advantages such as mild temperature conditions,high yields.All the novel benzoylphenylureas compounds were confirmed by spectroscopic methods including IR,1H NMR,13C NMR and HRMS. |
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| Keywords: | benzoylphenylureas chitin inhibitors synthesis |
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