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| 古陶瓷的XRF熔融玻璃片法测定 | |
| 引用本文： | 朱剑,毛振伟,张仕定,樊昌生,周广明,王昌燧.古陶瓷的XRF熔融玻璃片法测定[J].中国科学技术大学学报,2006,36(10):1101-1105. |
| 作者姓名： | 朱剑 毛振伟 张仕定 樊昌生 周广明 王昌燧 |
| 作者单位： | 1. 中国科学技术大学科技考古研究室,安徽合肥,230026;中国科学院研究生院人文学院科技史与科技考古系,北京,100049 2. 中国科学技术大学科技考古研究室,安徽合肥,230026 3. 中国科学技术大学合肥微尺度物质科学国家实验室(筹)安徽合肥,230026 4. 江西省文物考古研究所,江西南昌,330025 |
| 基金项目： | 国家自然科学基金;中国科学院知识创新工程项目;面向21世纪教育振兴行动计划(985计划) |
| 摘 要： | 针对古陶瓷测试标本一般较小,而测量精度要求较高的特点,将熔融玻璃片法应用于古陶瓷样品的分析之中,探讨了合适的实验条件.XRF面扫描分析的数据表明,熔片样品不同部位的Si、Al等主量元素,其分析线强度相对标准偏差均小于0.3%.4个商代原始瓷样品XRF测试结果与ICP-AES分析相应的数据颇为吻合.玻璃熔片均匀度好、试样用量少、保存时间长. |
| 关 键 词： | 原始瓷 面扫描 定量分析 |
| 文章编号： | 0253-2778(2006)10-1101-05 |
| 收稿时间： | 03 5 2006 12:00AM |
| 修稿时间： | 04 30 2006 12:00AM |
Ancient porcelain determination with fusion beads method by XRF |
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| ZHU Jian,MAO Zhen-wei,ZHANG Shi-ding,FAN Chang-sheng,ZHOU Guang-ming,WANG Chang-sui.Ancient porcelain determination with fusion beads method by XRF[J].Journal of University of Science and Technology of China,2006,36(10):1101-1105. | |
| Authors: | ZHU Jian MAO Zhen-wei ZHANG Shi-ding FAN Chang-sheng ZHOU Guang-ming WANG Chang-sui |
| Institution: | 1. Department of Science History and Archaeometry , University of Science and Technology of China, Hefei 230026,China; 2. Graduate University of the Chinese Academy of Sciences, Beijing 100049 ,China; 3. Hefei National Laboratory for Physical Science at the Microscale ,University of Science and Technology of China, Hefei 230026,China; 4. Institute of Culture Relic and Archaeology of Jiangxi Province, Nanchang 330025, China |
| Abstract: | Fusion beads method by X-ray fluorescence(XRF) was used to determinate bodies of ancient porcelain,which has been used for over forty years and has been proved to be a stable and efficient method in X-ray fluorescence analysis.Fusion beads application to ancient porcelain determination was discussed and the favorable conditions were obtained from the experiments.Si,Al and other components in different place of fusion beads were measured with X-ray fluorescence map scanning analysis and the standard deviation was less than 0.3%.Comparison of the components with Inductively Coupled Plasma Atomic Emission Spectrometry results indicates that this method is suitable for determining ancient porcelain. |
| Keywords: | WDXRF |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |