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| 基底预处理对于水热法制备ZnO微/纳米管阵列的影响 | |
| 引用本文： | 刘政楠,郭潇,郭敏,张梅. 基底预处理对于水热法制备ZnO微/纳米管阵列的影响[J]. 北京科技大学学报, 2011, 33(6): 756-761 |
| 作者姓名： | 刘政楠 郭潇 郭敏 张梅 |
| 作者单位： | 北京科技大学冶金与生态工程学院,北京,100083 |
| 基金项目： | 国家自然科学基金资助项目(No.50872011,No.50772004); 国家重点基础研究发展计划资助项目(No.2007CB613608); 教育部新世纪优秀人才支持计划资助项目(No.NCET-08-0723) |
| 摘 要： | 采用水热法系统研究了基底预处理(基底铺膜、不铺膜吹氮气处理和盐酸浸泡处理等)方式对于制备ZnO微/纳米管阵列的影响;结合ZnO晶体的微观结构,探讨了基底特征与ZnO微/纳米管阵列生长的内在联系.结果表明,采用高纯氮气和盐酸浸泡预处理基底均能制备得到ZnO微/纳米管阵列,并且这两种预处理方法制备出的纳米管在尺寸、形貌和分布上有所不同.ZnO微/纳米管成管机理研究表明,ZnO顶部锌终端对于生长微/纳米管起着决定性作用. |
| 关 键 词： | 氧化锌 纳米管阵列 基底 水热法 |
Effect of substrate pretreatments on the growth of ZnO micro/nanotube arrays by a hydrothermal method |
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| LIU Zheng-nan,GUO Xiao,GUO Min,ZHANG Mei. Effect of substrate pretreatments on the growth of ZnO micro/nanotube arrays by a hydrothermal method[J]. Journal of University of Science and Technology Beijing, 2011, 33(6): 756-761 | |
| Authors: | LIU Zheng-nan GUO Xiao GUO Min ZHANG Mei |
| Affiliation: | LIU Zheng-nan,GUO Xiao,GUO Min Wingdingsj,ZHANG Mei School of Metallurgical and Ecological Engineering,University of Science and Technology Beijing,Beijing 100083,China |
| Abstract: | The effects of substrate pretreatments,such as modifying the substrate with ZnO nanoparticles,drying the substrate with highly pure nitrogen and soaking the substrate with hydrochloric acid,on the growth of ZnO micro/nanotube arrays were systematically investigated by using a hydrothermal method.The relationship between substrate surface characteristics and the growth of ZnO micro/nanotube arrays was discussed based on ZnO microstructure.It is indicated that ZnO micro/nanotube arrays with different sizes,mo... |
| Keywords: | zinc oxide nanotube arrays substrates hydrothermal method |
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