The synthesis of a new cyclodextrin-crown ether chiral stationary phase and application in gas chromatography |
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Authors: | Liu Min Zeng Zhaorui Ding Yuqiang Liu Suhuai |
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Institution: | (1) College of Chemisty, Wuhan University, 430072 Wuhan, China;(2) Experiment Center of Nan-Yang College of Science and Technolegy, 473066 Nanyang, China |
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Abstract: | A new compound of mono-6-(1′-benzo-aza-15-crown-5)-2, 3, 6-permethyl-β-cyclodextrin (BA-15C5-PM-CD) was synthesized. The structure
was determined to be coincide with our anticipation by spectroscopy. As a stationary phase for capillary gas chromatography,
excellent separation for enantioners and positional isomers was achieved.
Supported by the National Natural Science Foundation of China(No. 29475201)
Liu Min: born in 1974, Graduate student |
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Keywords: | cyclodextrin-crown ether gas chromatography chiral stationary phase |
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