| CoPc(β-OC6Cl5)4/SnO2复合材料的制备及表征 |
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| 引用本文： | 尹彦冰,孙季如,任卉蕾,牟海涛.CoPc(β-OC6Cl5)4/SnO2复合材料的制备及表征[J].高师理科学刊,2012(2):53-55. |
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| 作者姓名： | 尹彦冰 孙季如 任卉蕾 牟海涛 |
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| 作者单位： | 齐齐哈尔大学化学与化学工程学院 |
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| 基金项目： | 黑龙江省普通高等学校青年学术骨干支持计划项目(1153G052) |
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| 摘 要： | 采用原位合成的方法制备CoPc(β-OC6Cl5)4/SnO2复合材料,利用UV,IR,XRD对产物进行表征.结果表明,CoPc(β-OC6Cl5)4/SnO2复合材料在紫外光谱中出现了酞菁特征吸收Q带的红移,红外光谱中出现了M-O的振动吸收峰,并且在XRD图谱中显现出SnO2晶粒变小,这说明CoPc(β-OC6Cl5...
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| 关 键 词： | 原位合成 复合材料 二氧化锡 |
Preparation and characteration of β-tetra-pentachlorophenyloxy-Cobalt Phthalocyanine/SnO2 nanocomposite |
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| YIN Yan-bing,SUN Ji-ru,REN Hui-lei,MU Hai-tao.Preparation and characteration of β-tetra-pentachlorophenyloxy-Cobalt Phthalocyanine/SnO2 nanocomposite[J].Journal of Science of Teachers＇College and University,2012(2):53-55. |
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| Authors: | YIN Yan-bing SUN Ji-ru REN Hui-lei MU Hai-tao |
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| Institution: | (School of Chemistry and Chemical Engineering,Qiqihar University,Qiqihar 161006,China) |
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| Abstract: | β-tetra-pentachlorophenyloxy-Cobalt Phthalocyanine/SnO2 nanocomposite were synthesized by in-situ process.The products were characterized by means of UV,IR and XRD methods.The experimental results indicate that different degree of red shift on the Q band with maximum absorption of the substitute phthalocyanine occurred,the vibration absorption peaks of M-O appreared in IR spectrum,and the size of crystal particals have become smaller than before in XRD spectrum,all that show the complex of tetra-pentachlorophenyloxy Cobalt Phthalocyanines and SnO2were linked with partial chemical bond. |
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| Keywords: | in-situ method composite SnO2 |
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