| 液相色谱法测定双酚A工艺物料中苯酚和高沸点物的含量 |
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| 引用本文： | 蔡威,毛细娥,周俊,汪星.液相色谱法测定双酚A工艺物料中苯酚和高沸点物的含量[J].沈阳大学学报,2007,19(6):46-51. |
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| 作者姓名： | 蔡威 毛细娥 周俊 汪星 |
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| 作者单位： | 1. 黑龙江省教育学院,黑龙江哈尔滨,150000
2. 惠州忠信化工有限公司,广东惠州,516082 |
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| 摘 要： | 研究了一种用液相色谱法测定双酚A物料中苯酚和高沸点物含量的方法.样品用乙腈溶解,经稀释后注入液相色谱仪中,以C18柱,乙腈/甲醇/水流动相梯度洗脱进行分离,紫外光度检测器检测,校正归一法定量.
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| 关 键 词： | 液相色谱 双酚A 苯酚 高沸点物 |
| 文章编号： | 1008-9225（2007）06-0046-06 |
| 收稿时间： | 2007-09-14 |
| 修稿时间： | 2007年9月14日 |
Liquid Chromatography Method Determination of Phenol and High boiling Components in Bisphenol A Process |
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| CAI Wei,MAO Xi'e,ZHOU Jun,WANG Xing.Liquid Chromatography Method Determination of Phenol and High boiling Components in Bisphenol A Process[J].Journal of Shenyang University,2007,19(6):46-51. |
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| Authors: | CAI Wei MAO Xi'e ZHOU Jun WANG Xing |
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| Abstract: | A liquid chromatography method determination of phenol and high-boiling components in bisphenol A process is investigated.The test sample is solved into acetonitrile.After dilution,the treated sample is injected to C18 column,separated using acetonitrile,methanol and water as fluid phase,detected by ultraviolet absorption detector.The detected data are quantized using correction and normalization methods. |
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| Keywords: | liquid chromatography bisphenol A phenol high-boiling component |
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