| 双杂原子Ti-Mn-ZSM-5分子筛的合成与表征 |
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| 引用本文： | 霍丽华,赵经贵,马淑杰. 双杂原子Ti-Mn-ZSM-5分子筛的合成与表征[J]. 黑龙江大学自然科学学报, 2000, 17(4): 65-67 |
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| 作者姓名： | 霍丽华 赵经贵 马淑杰 |
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| 作者单位： | 黑龙江大学化学化工学院,黑龙江哈尔滨 150080;吉林大学化学系,吉林长春 130023 |
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| 基金项目： | 黑龙江省自然科学基金资助课题(9732) |
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| 摘 要： | 在无碱性离子存在下,以硅溶胶、硫酸钛、硫酸锰为原料,分别采用四丙基溴化胺(TPABr)、1,6-己二胺(1,6-HDA)及正丁胺(R-NH2)模板剂,首次合成了双杂原子Ti-Mn-ZSM-5分子筛,并对产物的物性与结构进行了表征。
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| 关 键 词： | 双杂原子 Ti-Mn-ZSM-5分子筛 水热合成 |
| 文章编号： | 1001-7011(2000)04-0065-03 |
| 修稿时间： | 1999-11-20 |
Synthesis and characterization of zeolite Ti- Mn-ZSM-5 containing double heteroatoms |
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| HUO Li-Hua,ZHAO Jing-Gui,MA Shu-jie. Synthesis and characterization of zeolite Ti- Mn-ZSM-5 containing double heteroatoms[J]. Journal of Natural Science of Heilongjiang University, 2000, 17(4): 65-67 |
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| Authors: | HUO Li-Hua ZHAO Jing-Gui MA Shu-jie |
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| Abstract: | In the absence of alkali metal ions, the zeolite Ti-Mn-ZSM-5 containing double heteroatom, with silica sol as Si sources, titanium sulfate and manganese sulfate as the starting materials and tetrapropyl ammomium bromide(TPABr), 1, 6-dihexamine(l, 6-HDA) and n-butylamine (R-NH2) as the templates, respectively, was synthesized for the first time. Some physical and chemical properties and the structure of the product were characterized by using XRD, SEM, TG-DTA, IR and ESR methods. |
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| Keywords: | double heteroatom Ti-Mn-ZSM-5 zeolite hydrothermal synthesis |
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