| 三氯化磷催化合成氯乙酸异丙酯 |
| |
| 引用本文： | 梁春根 林原斌. 三氯化磷催化合成氯乙酸异丙酯[J]. 湘潭大学自然科学学报, 1997, 19(2): 49-50 |
| |
| 作者姓名： | 梁春根 林原斌 |
| |
| 作者单位： | 湘潭大学化学化工学院!湘潭，411105 |
| |
| 摘 要： | 以三氯化磷为催化剂，氯乙酸和异而醇反应合成氯乙酸异雨酯，收率为89．5％，纯度为98％．该反应时间短，可以避免浓硫酸带来的腐蚀问题，反应的后处理简单．
|
| 关 键 词： | 三氯化磷 氯乙酸异丙酯 异丙醇 氯乙酸 合成 |
THE SYNTHESIS OF ISOPROPYL CHLOROACETATE BY PHOSPHORUS TRICHLORIDE CATALYST |
| |
| Liang Chungen, Lin Yuanbin, Shen Dongshen. THE SYNTHESIS OF ISOPROPYL CHLOROACETATE BY PHOSPHORUS TRICHLORIDE CATALYST[J]. Natural Science Journal of Xiangtan University, 1997, 19(2): 49-50 |
| |
| Authors: | Liang Chungen Lin Yuanbin Shen Dongshen |
| |
| Abstract: | The synthesis of isopropyl chloroacetate from chloroacetic acid with isopropanol in the presence of phosphorus- trichloride was reported in this opaper. The influence of reaction condition on yield was studied. The reaction time is short. The yield is 89. 5% with 98% (GC) purity. This method can avoid the corrosive problem caused by the sulfuric acid and the after - treatment is simple. |
| |
| Keywords: | phosphorus-trichloride isopropyl chloroacetate isopropanol chloroacetic acid synthesis |
| 本文献已被 CNKI 维普 等数据库收录！ |
