| 冬枣中果糖、葡萄糖、蔗糖的高效液相色谱分析 |
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| 引用本文： | 王庭欣,陈永刚,张晓瑜,夏立娅,李小亭.冬枣中果糖、葡萄糖、蔗糖的高效液相色谱分析[J].河北大学学报(自然科学版),2012,32(5):528-531. |
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| 作者姓名： | 王庭欣 陈永刚 张晓瑜 夏立娅 李小亭 |
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| 作者单位： | 1. 河北大学质量技术监督学院,河北保定,071000
2. 黄骅市质量技术监督局食品质量安全监督检验中心,河北黄骅,061100 |
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| 基金项目： | 质检公益性行业科研专项基金资助项目(200810345-2) |
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| 摘 要： | 为建立冬枣中果糖、葡萄糖、蔗糖的高效液相色谱分析方法,以C18柱为分离柱进行色谱分析.色谱条件为:流动相V(乙腈)∶V(水)=80∶20,流速1.4mL/min,柱温35℃.样品加标回收率为96%～102%,相对标准偏差小于2.7%.本方法具有回收率高、灵敏度高、精密度高等优点,适用于冬枣中果糖、葡萄糖、蔗糖的检测。
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| 关 键 词： | 高效液相色谱 果糖 葡萄糖 蔗糖 冬枣 |
Analysis of fructose,glucose and sucrose in Zizyphus jujube Mill.cv by high performance liquid chromatographic |
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| WANG Tingxin
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CHEN Yonggang
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ZHANG Xiaoyu
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XIA Liya
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LI Xiaoting.Analysis of fructose,glucose and sucrose in Zizyphus jujube Mill.cv by high performance liquid chromatographic[J].Journal of Hebei University (Natural Science Edition),2012,32(5):528-531. |
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| Authors: | WANG Tingxin CHEN Yonggang ZHANG Xiaoyu XIA Liya LI Xiaoting |
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| Institution: | 1(1.College of Quality and Technical Supervision,Hebei University,Baoding 071000,China; 2.Food Quality Safety Supervision and Inspection Center,Huanghua Administration of Quality Technology Supervision,Huanghua 061100,China) |
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| Abstract: | A high performance liquid chromatographic method was developed to determine of fructose,glucose and sucrose in Zizyphus jujube Mill.cv.The method was adopted with acetonitrile and water(80∶20,V∶V) as the eluent.The flow rate was 1.4 mL/min and column temperature 35 ℃.The recovery rate was in 96%-102% range and the relative standard deviation below 2.7%.This method is simple,accurate and suitable for the determination of fructose,glucose and sucrose in Zizyphus jujube Mill.cv. |
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| Keywords: | HPLC fructose glucose sucrose Zizyphus jujube Mill cv |
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