| 过氧化氢氧化－水热结晶联合法制备高纯MoO_3粉末 |
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| 引用本文： | 钱逸泰,陈波,王成云,谢毅,陈祖耀,周贵恩,陆斌,范成高.过氧化氢氧化－水热结晶联合法制备高纯MoO_3粉末[J].中国科学技术大学学报,1994(1). |
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| 作者姓名： | 钱逸泰 陈波 王成云 谢毅 陈祖耀 周贵恩 陆斌 范成高 |
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| 摘 要： | 首次使用过氧化氢氧化－水热结晶联合法制备了高纯ＭＯＯ３粉末．对其粉末粒子的尺寸、形貌和结晶习性进行了研究，对其纯度进行发射光谱分析，并对水热结晶的过程提出了一个可能的机理．
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| 关 键 词： | MoO_3粉末，水热结晶，过氧化氢氧化 |
Preparation of Pure MoO_3 Powder by H_2O_2 Oxidation Hydrothermal Crystallization Combined Method |
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| Qian Yitai, Chen Bo, Wang Chengyun,Xie Yi ,Chen Zuyao.Preparation of Pure MoO_3 Powder by H_2O_2 Oxidation Hydrothermal Crystallization Combined Method[J].Journal of University of Science and Technology of China,1994(1). |
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| Authors: | Qian Yitai Chen Bo Wang Chengyun Xie Yi Chen Zuyao |
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| Institution: | Qian Yitai; Chen Bo; Wang Chengyun;Xie Yi ;Chen Zuyao(Department of Applied Chemistry )Zhou Guien; Lu Bing ;Fan Chenggao(Structure Research Laboratory ) |
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| Abstract: | H2O2 oblation-hydrothermal crystallization combined method was employed for the first time for the preparation of pure MoO3 powder. The particle she and crystal morphology are studied with XRD and TEM methods. The total content of main metallic hopurities is less than 14ppm. A possible gel crystallization mechanism is proposed. |
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| Keywords: | ?MoO_3 powder hydrothermal crystallization H_2O_2-oxidation |
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