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| 盐酸坦索罗辛的波谱学研究 | |
| 引用本文： | 刘英华,原现瑞,陈晓霞,李润岩. 盐酸坦索罗辛的波谱学研究[J]. 河北科技大学学报, 2008, 29(4): 320-324 |
| 作者姓名： | 刘英华 原现瑞 陈晓霞 李润岩 |
| 作者单位： | 河北科技大学河北省分析测试研究中心,河北石家庄,050018;河北科技大学化学与制药工程学院,河北石家庄,050018 |
| 摘 要： | 对盐酸坦索罗辛的红外光谱(FT-IR)、一维及二维核磁共振谱(1H NMR,13C NMR,DEPT,1H-1H COSY,HSQC,HMBC)进行了解析,对其所有的NMR谱信号进行了归属,讨论了红外特征吸收峰所对应的官能团的振动形式,确证了盐酸坦索罗辛的结构。 |
| 关 键 词： | 核磁共振 归属 2D NMR FT-IR 盐酸坦索罗辛 |
| 收稿时间： | 2008-05-12 |
| 修稿时间： | 2008-07-10 |
Structure elucidation of tamsulosin hydrochloride by FT-IR and NMR spectra |
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| LIU Ying-hu,YUAN Xian-rui,CHEN Xiao-xia and LI Run-yan. Structure elucidation of tamsulosin hydrochloride by FT-IR and NMR spectra[J]. Journal of Hebei University of Science and Technology, 2008, 29(4): 320-324 | |
| Authors: | LIU Ying-hu YUAN Xian-rui CHEN Xiao-xia LI Run-yan |
| Affiliation: | LIU Ying-hua1,YUAN Xian-rui1,CHEN Xiao-xia1,LI Run-yan2(1.Hebei Research Center of Analysis , Testing,Hebei University of Science , Technology,Shijiazhuang Hebei 050018,China,2.College of Chemical , Pharmaceutical Engineering,China) |
| Abstract: | The infrared spectrum,1D and 2D NMR(1H NMR,13C NMR,DEPT,1H-1H COSY,HSQC and HMBC) spectra of tamsulosin hydrochloride were reported and interpreted.All the NMR signals were assigned.The infrared spectrum was analyzed to derive the types of vibration of the functional groups.The structure of tamsulosin hydrochloride was elucidated. |
| Keywords: | 2D NMR FT-IR |
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