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食用花椒油化学成分的GC-MS分析
引用本文:石爱华,欧阳玉祝,李佑稷,陈小东,谢显华.食用花椒油化学成分的GC-MS分析[J].吉首大学学报(自然科学版),2008,29(2):101-105.
作者姓名:石爱华  欧阳玉祝  李佑稷  陈小东  谢显华
作者单位:(吉首大学化学化工学院,湖南 吉首 416000)
摘    要:用超声波辅助提取法从花椒籽核和壳中提取花椒油,用GC-MS联用仪对不同材料中提取的花椒油的化学成分进行了分析.实验结果表明:用超声辅助法从花椒籽核和皮中提取的油的提取率分别为7.8%和6.74%.成分分析表明花椒籽核和皮中提取的油化学成分差异很大.用极性溶剂提取时,籽核油主要成分是烯烃,烯烃含量占总含量的48.73%,油中未检出麻辣酰胺物质.花椒籽壳油主要成分是羧酸和羧酸酯,含量占总含量的66.45%,其中酰胺类物质含量为3.84%.

关 键 词:花椒油  成分  超声波  分析  
文章编号:1007-2985(2008)02-0101-05
修稿时间:2008年1月26日

Chemical Constitute Analysis of the Food Oil from Zanthorylum Bungeanum by GC-MS
SHI Ai-hua,OUYANG Yu-zhu,LI You-ji,CHEN Xiao-dong,XIE Xian-hua.Chemical Constitute Analysis of the Food Oil from Zanthorylum Bungeanum by GC-MS[J].Journal of Jishou University(Natural Science Edition),2008,29(2):101-105.
Authors:SHI Ai-hua  OUYANG Yu-zhu  LI You-ji  CHEN Xiao-dong  XIE Xian-hua
Institution:(College of Chemistry and Chemical engineering,Jishou University,Jishou 416000,Hunan China)
Abstract:The conditions for ultrasonic extracting oil from Zanthorylum bungeanum nucleus and shuck were studied.Chemical constitute of oil from Zanthorylum bungeanum nucleus and shuck were analyzed by GC-MS.The experimental results show that the extract yield of Zanthorylum bungeanum oil from nucleus and shuck is 7.8% and 48.9%,respectively.Constitute analysis shows that chemical constitutes of oil from nucleus and shuck and different.Constitute of oil by polar solvent extraction from nucleus is olefin,and its percentage concentration is 48.73%,no acidamide substance in oil.Constitute of oil by polar solvent extraction from shuck is carboxylic acid and carboxylic ester,and its percentage concentration is 66.45%,acidamide substance percentage concentration is 3.84%.
Keywords:zanthorylum bungeanum oil  constitute  ultrasonic wave  analysis
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