| 新型阻燃剂磷酸三(五氯苯)酯的合成研究 |
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| 引用本文： | 朱广军,张熙和,邹运湖.新型阻燃剂磷酸三(五氯苯)酯的合成研究[J].南京理工大学学报(自然科学版),1993(3). |
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| 作者姓名： | 朱广军 张熙和 邹运湖 |
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| 作者单位： | 华东工学院化工学院
(朱广军，张熙和)，华东工学院化工学院(邹运湖) |
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| 摘 要： | 该文提出了以苯或甲苯为溶剂,用吡啶吸收氯化氢,由五氯酚和POCl_3反应合成磷酸三(五氯苯)酯的合成路线,经实验发现了影响反应的因素,反应的得率可达到80％。用涂层法测定阻燃效果,显示磷酸三(五氯苯)酯是一种较好的新型阻燃剂。
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| 关 键 词： | 阻燃剂 五氯酚 合成试验 磷酸酯 |
Synthesis Study of a New Flame Retardant Tris (Pentachlorophenyl) Phosphate |
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| Zhu Guangjun Chemical Engineering School.Synthesis Study of a New Flame Retardant Tris (Pentachlorophenyl) Phosphate[J].Journal of Nanjing University of Science and Technology(Nature Science),1993(3). |
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| Authors: | Zhu Guangjun Chemical Engineering School |
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| Institution: | Zhu Guangjun Chemical Engineering School |
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| Abstract: | A new synthesis method of tris (pentachlorophenyl)phosphate from pentachlorophenol and POCl_3 is proposed, which usesbenzene or toluene as solvent and pyridine to absorb HCl. The yieldreached 80%. The factors which influence the reaction were studied.The flame retarding effect was tested by coating method. It showedtris (pentachlorophenyl) phosphate is a new good flame retardant. |
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| Keywords: | flame retardant pentachlorophenol synthetic tests phosphate |
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