| 4,5-二硫代亚乙基-1,3-二硫代环戊烯-2-酮和硫酮衍生物的合成 |
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| 引用本文： | 赵卫国,伍维成,沈永嘉.4,5-二硫代亚乙基-1,3-二硫代环戊烯-2-酮和硫酮衍生物的合成[J].华东理工大学学报(自然科学版),1997(5). |
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| 作者姓名： | 赵卫国 伍维成 沈永嘉 |
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| 作者单位： | 华东理工大学精细化工研究所 |
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| 摘 要： | 合成了文题化合物及它们的酯化物，给出了它们的核磁共振氢谱和质谱。讨论了影响反应的一些因素，比较了不同溴代试剂与锌酸盐发生反应的活泼性。
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| 关 键 词： | 羟基取代 酯化反应 四硫代富瓦烯 合成金属 1，3－二硫代环戊－2－酮 |
Synthesis of 4,5 Ethylenedithio 1,3 dithiole 2 one and Thione Derivatives |
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| Zhao Weiguo,Wu Weichen and Shen Yongjia.Synthesis of 4,5 Ethylenedithio 1,3 dithiole 2 one and Thione Derivatives[J].Journal of East China University of Science and Technology,1997(5). |
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| Authors: | Zhao Weiguo Wu Weichen and Shen Yongjia |
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| Institution: | Zhao Weiguo,Wu Weichen and Shen Yongjia * |
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| Abstract: | Several hydroxyl substituted 4,5 ethylenedithio 1,3 dithiole 2 one and thiones and their ester derivatives were synthesised. Their 1H NMR and MS data were given. The factors of affecting on the reaction were discussed and the reaction activities of various bromo hydrocarbons reaction with zincate were given. |
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| Keywords: | hydroxyl substituent esterification tetrathiafulvalene synthetic metals 1 3 dithiole 2 one |
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