| 微波消解石墨炉法检测龟甲胶中铬元素含量简 |
| |
| 引用本文： | 王蓉,施志顺,史学礼,周至美,耿武松,益磊,李志华.微波消解石墨炉法检测龟甲胶中铬元素含量简[J].菏泽学院学报,2013(5):60-63. |
| |
| 作者姓名： | 王蓉 施志顺 史学礼 周至美 耿武松 益磊 李志华 |
| |
| 作者单位： | [1]毫州职业技术学院药学院,安徽毫州236800 [2]毫州市食品药品检验所,安徽亳州236800 [3]岛津企业管理（中国）有限公司,广东广州510000 |
| |
| 摘 要： | 通过以下方法对龟甲胶中的铬进行检测：龟甲胶样品经微波消解后，采用石墨炉原子吸收分光光度法测定铬含量．结果表明，铬在0～12．5μg/L范围内与吸光度呈良好线性关系，相关系数r=0．9986，检出限为1．58ng／mL，平均加标回收率为94．8％．因此，认为这种方法可满足龟甲胶中微量铬含量的测定．
|
| 关 键 词： | 龟甲胶 铬 检测 微波消解 石墨炉 |
Determination of Chromium in Tortoise - shell Glue by Graphite Furnace with Microwave digestion |
| |
| Institution: | WANG Rong SHI Zhi -shun SHI Xue- li ZHOU Zhi- mei GENG Wu- song YI Lei LI Zhi -hua ( 1. College of Pharmacy, Bozhou Vocational and technical College, Bozhou Anhui 236800,China; 2. Bozhou Institute for Food And Drug Contro, Bozhou Anhui 236800, China; 3. SHIMADZU Enterprise Management (China) Co. , Ltd. , Guangzhou Guangdong 510000, China) |
| |
| Abstract: | To detect the chromium in the tortoise - shell glue through the following methods： tortoise - shell glue samples by microwave digestion, spectrophotometry for determination of chromium content by graphite furnace atomic absorption. The results show that, chromium in 0 ~ 12.5 μg/L showed a good linear relationship with theabsorbance range, the correlation coefficient r =0.998 6, the detection limit is 1.58 ng/mL, the average recovery is 94.8%. Therefore, this method can meet the determination of chromium content in the tortoise - shell glue. |
| |
| Keywords: | tortoise - shell glue meet the determination of chromium content in the tortoise -shell glue chromium test microwave digestion graphite furnace |
| 本文献已被 CNKI 维普 等数据库收录！ |
|
