| 马钱苷的NMR数据解析 |
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| 引用本文： | 范毅,张海艳,李坤威,张剑,赵天增.马钱苷的NMR数据解析[J].河南科学,2014(9):1703-1705. |
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| 作者姓名： | 范毅 张海艳 李坤威 张剑 赵天增 |
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| 作者单位： | 1. 河南省生物技术开发中心,郑州,450002
2. 河南省生物技术开发中心，郑州 450002; 中国标准化研究院，北京 100010 |
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| 基金项目： | 质检公益性行业科研专项经费资助项目 |
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| 摘 要： | 通过DEPT及1H-1HCOSY,HSQC,HMBC,NOESY等2D NMR技术,对环烯醚萜苷化合物——马钱苷的1H和13CNMR信号进行了详细解析和全归属,尤其利用NOESY技术确证了其立体结构.
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| 关 键 词： | NMR 归属 NOESY 马钱苷 |
An NMR Study on Chrysathain |
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| Fan Yi,Zhang Haiyan,Li Kunwei,Zhang Jian,Zhao Tianzeng.An NMR Study on Chrysathain[J].Henan Science,2014(9):1703-1705. |
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| Authors: | Fan Yi Zhang Haiyan Li Kunwei Zhang Jian Zhao Tianzeng |
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| Institution: | Fan Yi, Zhang Haiyan, Li Kunwei, Zhang Jian, Zhao Tianzeng (1. Biotechnoiogy Developing Center, Henan Academy of Sciences, Zhengzhou 450002, China; 2. China National Institute of Standardization, Beijing 100010, China ) |
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| Abstract: | Loganin,an important iro doid,was usually isolated from Cornus officinalis Sieb,et Zucc. and Lonicera chrysatha Thunb.. The 1H and 13C NMR chemical shifts of loganin were completely assigned by using a combination of ^1D NMR（^1H,^13C NMR and DEPT）and 2D NMR（^1H- ^1H COSY,HSQC,HMBC and NOESY）techniques, especially its stereoscopic strcture was studied with NOESY. |
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| Keywords: | NMR assignment NOESY loganin |
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