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气/质联用测定大气飘尘之多环芳烃
引用本文:何立坚,章汝平.气/质联用测定大气飘尘之多环芳烃[J].龙岩学院学报,2007,25(3):63-65.
作者姓名:何立坚  章汝平
作者单位:1. 厦门海洋职业技术学院,福建厦门,361006;厦门唯希雅押花礼品有限公司,福建厦门,361100
2. 龙岩学院化学与材料工程系,福建龙岩,364000
基金项目:福建省自然科学基金,福建省教育厅科研项目
摘    要:通过提取方法、升温程序、色谱分离温度、载气流速等的优化,气/质(GC/MS)联用测定大气飘尘所含19种多环芳烃,快速、灵敏,检测限可达到0.02ng/mL,不失为一具有价值的分析方法.以此法同时测得龙岩市区大气飘尘样中菲、萘、(茁)、惹烯含量较高,美国EPA优先控制的有毒有害的多环芳烃物种也均有检出,值得关注.

关 键 词:气相色谱/质谱(GC/MS)  大气飘尘  多环芳烃
文章编号:1673-4629(2007)03-0063-03
收稿时间:2006-12-25
修稿时间:2006-12-25

Determination of Polycyclic Aromatic Hydrocarbons in Airborne Particulate by Gas Chromatography/Mass Spectrometry
HE Li-jian,ZHANG Ru-ping.Determination of Polycyclic Aromatic Hydrocarbons in Airborne Particulate by Gas Chromatography/Mass Spectrometry[J].Journal of Longyan Univercity,2007,25(3):63-65.
Authors:HE Li-jian  ZHANG Ru-ping
Abstract:By optimizing extracting method,heating procedure,chromatographic temperature,19 polycyclic aromatic hydrocarbons in airborne particulate are detected by gas chromatography/mass spectrometry(GC/MS) with quickness and good sensitiveness.The detect limit is be 0.02ng/mL.It is a valuable analysis method.By this method,the concentration of phenanthrene,naphthalene and retene is found relatively high in airborne particulate in Longyan City.Some toxic polycyclic aromatic hydrocarbons controlled by EPA are also detected.
Keywords:gas chromatography/mass spectrometry(GC/MS)  airborne particulate  polycyclic aromatic hydrocarbons
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