| 无水三氯化铝催化合成乙酸环己酯 |
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| 引用本文： | 孙婷,刘淑娟,赵进行.无水三氯化铝催化合成乙酸环己酯[J].淮阴师范学院学报(自然科学版),2005,4(3):228-230. |
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| 作者姓名： | 孙婷 刘淑娟 赵进行 |
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| 作者单位： | 许昌学院,化学系,河南,许昌,461000 |
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| 基金项目： | 河南省高校青年骨干教师基金资助项目（189）. |
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| 摘 要： | 以无水三氯化铝为催化剂,以冰乙酸和环己醇为原料合成乙酸环己酯.研究了酯化反应的影响因素,优化反应条件为:n(乙酸)=0.2 mol,n(环己醇)∶n(乙酸)=1.5∶1,催化剂用量1.5 g,反应时间45 min,带水剂环己烷10 mL,酯化率(以冰乙酸计)达95.9%.
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| 关 键 词： | 乙酸环己酯 催化 无水三氯化铝 |
| 文章编号： | 1671-6876（2005）03-0228-03 |
| 收稿时间： | 2005-03-08 |
| 修稿时间： | 2005年3月8日 |
Study on the Synthesis of Cyclohexyl Acetate Catalyzed by Anhydrous Aluminum Chloride |
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| SUN Ting,LIU Shu-juan,ZHAO Jin-xing.Study on the Synthesis of Cyclohexyl Acetate Catalyzed by Anhydrous Aluminum Chloride[J].Journal of Huaiyin Teachers College(Natrual Science Edition),2005,4(3):228-230. |
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| Authors: | SUN Ting LIU Shu-juan ZHAO Jin-xing |
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| Abstract: | Cyclohexyl acetate was synthesized from acetic acid and cyclohexanol with anhydrous aluminum chloride as catalyst. The factors influencing the esterification were studied. The optimized conditions are: n(acetic acid)=0.2mol, n(cyclohexanol): n(acetic acid)=1.5:1(the molar ratio), the amount of anhydrous aluminum chloride=1.5g, the reaction time 45min. yield of cyclohexyl acetate is 95.9% (based on acetic acid). |
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| Keywords: | cyclohexyl acetate catalysis anhydrous aluminum chloride |
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