| 自组装固定相反相HPLC聚合物柱的制备 |
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| 引用本文： | 陈福南,章竹君.自组装固定相反相HPLC聚合物柱的制备[J].西南师范大学学报(自然科学版),2002,27(3):364-367. |
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| 作者姓名： | 陈福南 章竹君 |
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| 作者单位： | 西南师范大学化学化工学院,重庆,400715 |
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| 基金项目： | 重庆市科技攻关项目“蛋白质及肽类药物的分离分析”资助 |
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| 摘 要： | 报道了一种自组装固定相的HPLC聚合物柱。苯乙烯，二乙烯苯，Victgo2100和稀释剂反应形成多孔微粒，这些微粒的表面覆盖了一层Victo2100的中间脂肪段，这一层C18膜就是固定相。本方法制备的HPLC柱分离芳香族化合物，柱效高而压力低。
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| 关 键 词： | 自组装固定相 HPLC 反相高效液相色谱法 聚合物柱 碳18膜 苯乙烯 二乙烯苯 Victo2100 |
The Preparation of Polymer Column for HPLC Using Self-assembling Stationary Phase |
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| CHEN Fu nan,ZHANG Zhu jun School of Chemisty and Chemical Enginering,Southwest China Normal University,Chongqing ,China.The Preparation of Polymer Column for HPLC Using Self-assembling Stationary Phase[J].Journal of Southwest China Normal University(Natural Science),2002,27(3):364-367. |
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| Authors: | CHEN Fu nan ZHANG Zhu jun School of Chemisty and Chemical Enginering Southwest China Normal University Chongqing China |
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| Institution: | CHEN Fu nan,ZHANG Zhu jun School of Chemisty and Chemical Enginering,Southwest China Normal University,Chongqing 400715,China |
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| Abstract: | The polymer column for HPLC using self assembling stationary phase has been developed. The styrene, divinylbenzene,Victo 2100 and diluent to form uniform connected non porous spheres. These polystyrene divinylbenzene spheres were coated with the aliphatic middle block of Victo 2100, which serve as the stationary phase . The present column were used to separate aromatic carbohydrate with high column efficiencies and low back pressure. |
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| Keywords: | High Performance Liquid Chromatography(HPLC) stationary phase polymer column |
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