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基于PCS的纳米颗粒粒度测量系统设计
引用本文:彭善琼.基于PCS的纳米颗粒粒度测量系统设计[J].吉首大学学报(自然科学版),2014,35(4):34-42.
作者姓名:彭善琼
作者单位:(湖南第一师范学院,湖南 长沙 410205)
基金项目:湖南省自然科学基金资助项目(11JJ6060)
摘    要:引入不同孔径的光纤传输激光和散射光子,不同孔径的Y形光纤传输入射光和散射光,采用光子相关光谱法(PCS)设计了纳米颗粒测量系统.讨论了光纤芯径、显微物镜的数值孔径、温度和散射角度对测量结果的影响.实验结果表明,温度在13~22℃超净间中,该系统能准确地测量纳米颗粒粒度.

关 键 词:光子相关光谱法(PCS)  纳米颗粒  测量系统  单分散体系  双分散体系

Development of Nano-Particle Measurement System Based on Photon Correlation Spectroscopy
PENG Shanqiong.Development of Nano-Particle Measurement System Based on Photon Correlation Spectroscopy[J].Journal of Jishou University(Natural Science Edition),2014,35(4):34-42.
Authors:PENG Shanqiong
Institution:(Hunan First Normal University,Changsha 410205,China)
Abstract:Different aperture fiber were applied for transmission of laser and scattered photons, different aperture y-type fiber were used for transmission of incident and scattered light synchronously. Based on photon correlation spectroscopy the nanometer particle measuring system was designed. Besides, the af- fects of fiber core diameter, microscope objectives numerical aperture, temperature and scattering angle were discussed. Experiments show that it is accurate and stable for nano-particle size distribution meas- urement, all experiments were finished in super clean room,in which temperature was controlled at about 13-22 ℃.
Keywords:photon correlation spectroscopy (PCS)  nano-particles  measurement system  single scatteredsystem  double scattered system
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