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合成聚羧酸减水剂不饱和聚醚双键保留率的测定分析
引用本文:窦琳,王玲,赵婷婷,任建国,王自为.合成聚羧酸减水剂不饱和聚醚双键保留率的测定分析[J].山西大学学报(自然科学版),2011,34(1):110-113.
作者姓名:窦琳  王玲  赵婷婷  任建国  王自为
作者单位:山西大学化学化工学院,山西,太原,030006
基金项目:山西省科技攻关项目(2006031141)
摘    要:采用滴定分析法测定不饱和聚醚的双键保留率,以烯丙醇聚氧乙烯基醚为例,分析了影响其测定的多种因素.结果表明用该方法(乙酸汞与不饱和聚醚反应)测定不饱和聚醚双键保留率是非常实用的,并根据测定结果可知,取样多少以及试样的pH值对测定有影响.

关 键 词:不饱和聚醚  滴定分析  双键保留率  减水剂

Double Bonds Retention Rate of Unsaturated Polyether in PolycarbOxylate Superplasticizer
DOU Lin,WANG Ling,ZHAO Ting-ting,REN Jian-guo,WANG Zi-wei.Double Bonds Retention Rate of Unsaturated Polyether in PolycarbOxylate Superplasticizer[J].Journal of Shanxi University (Natural Science Edition),2011,34(1):110-113.
Authors:DOU Lin  WANG Ling  ZHAO Ting-ting  REN Jian-guo  WANG Zi-wei
Institution:DOU Lin,WANG Ling,ZHAO Ting-ting,REN Jian-guo,WANG Zi-wei(School of Chemistry and Chemical Engineering,Shanxi University,Taiyuan 030006,China)
Abstract:The double bonds retention rate of unsaturated polyether was determined by titrimetric analysis,moreover,taking polyoxyethylene allyl ethers for example,the many reasons effecting the determination results were dicussed.The results show that the method(the reaction of mercuric acetate and unsaturated polyether) was very useful in determining double bounds retention rate.The factors affecting determination results are the amount of different samples and different pH value.
Keywords:unsaturated polyether  titrimetry  the double bonds retention rate  superplasticizer  
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