除虫菊酯I的NMR数据解析 |
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引用本文: | 李坤威,;张剑,;张海艳,;徐西震,;赵天增.除虫菊酯I的NMR数据解析[J].河南科学,2014(7):1193-1196. |
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作者姓名: | 李坤威 ;张剑 ;张海艳 ;徐西震 ;赵天增 |
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作者单位: | [1]中国标准化研究院,北京100010; [2]河南省科学院生物技术开发中心,郑州450002 |
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基金项目: | 国家科技支撑计划资助(2012BAB18B04) |
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摘 要: | 从除虫菊酯中分离得到除虫菊酯I,通过DEPT及1H-1HCOSY,HSQC,HMBC,NOESY等2D NMR技术对该化合物所有的1H和13C NMR信号进行了详细解析和全归属.
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关 键 词: | NMR 归属 D NMR 除虫菊酯I |
An NMR Study on Pyrethrin I |
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Institution: | Li Kunwei, Zhang Jian, Zhang Haiyan, Xu Xizhen, Zhao Tianzeng (1. China National Institute of Standardization, Beijing 100010, China; 2. Biotechnoiogy Developing Center, Henan Academy of Sciences, Zhengzhou 450002, China) |
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Abstract: | Pyrethrin I was isolated from pyrethrins. The 1H and 13C NMR chemical shifts of the compounds were completely assigned using a combination of 1D NMR(IH, 13C NMR and DEPT) and 2D NMR(1H-1H COSY, HSQC, HMBC and NOESY) techniques. |
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Keywords: | NMR assignment 2D NMR PyrethrinI |
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