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Bi3TiNbO9压电陶瓷制备工艺研究
引用本文:刘丹,陈强,彭志航,肖定全,朱建国.Bi3TiNbO9压电陶瓷制备工艺研究[J].湖北大学学报(自然科学版),2013(2):173-175,184.
作者姓名:刘丹  陈强  彭志航  肖定全  朱建国
作者单位:四川大学材料科学与工程学院
基金项目:国家自然科学基金(61201064)资助
摘    要:以Bi3TiNbO9和TiO2为原料,采用固相法合成Bi3TiNbO9(BTN)压电陶瓷.用X线衍射仪和电子显微镜等对陶瓷样品进行分析.实验结果表明,采用固相法可在较低烧结温度下制备出单相的BTN陶瓷.探讨不同工艺参数对BTN压电陶瓷的压电、介电性能的影响.实验发现,较高的成型压强可以制得致密且均匀的BTN陶瓷.再结晶可以使晶粒生长均匀,且能够承受较高的极化场强.在8kV/mm场强下极化的BTN陶瓷的压电常数d33为5.6pC/N.

关 键 词:Bi3TiNbO9  铋层状铁电体  压电陶瓷

Research on processing of Bi3NbTiO9 piezoelectric ceramics
LIU Dan,CHEN Qiang,PENG Zhihang,XIAO Dingquan,ZHU Jianguo.Research on processing of Bi3NbTiO9 piezoelectric ceramics[J].Journal of Hubei University(Natural Science Edition),2013(2):173-175,184.
Authors:LIU Dan  CHEN Qiang  PENG Zhihang  XIAO Dingquan  ZHU Jianguo
Institution:(College of Materials Scienc and Engineering,Sichuan University,Chengdu 610064,China)
Abstract:Ceramic samples with the composition of Bi3TiNbO9(BTN) were prepared by solidstate reaction method and using Bi203 ,TiO2 and Nb205 as start materials. The samples were analyzed using X-ray diffraction and scan electron microscopy. It was found that BTN ceramics could be fabricated at lower sintering temperature and the different process conditions had the important influence on their piezoelectric and dielectric properties. The dense and uniform BTN ceramics could be obtained by isostatic pressure, according to the experiment. The recrystallization could make the ceramic grains grow uniformly and withstand higher polarization field. The d33 of BTN ceramics poled by 8 kV/mm was about 5.6 pC/N.
Keywords:Bi3TiNbO9  bismuth layer-structured ferroelectric  piezoelectric ceramics
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